Technology Process of C40H37F6N3O6
There total 9 articles about C40H37F6N3O6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
potassium carbonate;
In
N,N-dimethyl-formamide;
at 23 - 50 ℃;
for 8h;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: ammonium carbonate / ethanol / 72 h / 58 °C / Inert atmosphere
2: potassium carbonate / N,N-dimethyl-formamide / 8 h / 23 - 50 °C
With
ammonium carbonate; potassium carbonate;
In
ethanol; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: toluene-4-sulfonic acid / ethanol / 4 h / Reflux
2.1: dimethylsulfide borane complex / tetrahydrofuran / 18 h / 23 °C / Inert atmosphere
2.2: 18 h / 0 - 23 °C / Inert atmosphere
3.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 1 h / -78 °C / Inert atmosphere
4.1: ammonium carbonate / ethanol / 72 h / 58 °C / Inert atmosphere
5.1: potassium carbonate / N,N-dimethyl-formamide / 8 h / 23 - 50 °C
With
oxalyl dichloride; dimethylsulfide borane complex; ammonium carbonate; potassium carbonate; toluene-4-sulfonic acid; dimethyl sulfoxide;
In
tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide;