C₂₂H₂₂ClF₄N₅O₄S

Base Information

Chemical Name:C₂₂H₂₂ClF₄N₅O₄S
CAS No.:1613395-78-0
Molecular Formula:C₂₂H₂₂ClF₄N₅O₄S
Molecular Weight:563.96
Hs Code.:

C<sub>22</sub>H<sub>22</sub>ClF<sub>4</sub>N<sub>5</sub>O<sub>4</sub>S

Synonyms:C₂₂H₂₂ClF₄N₅O₄S

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Chemical Property of C₂₂H₂₂ClF₄N₅O₄S

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Technology Process of C₂₂H₂₂ClF₄N₅O₄S

There total 6 articles about C₂₂H₂₂ClF₄N₅O₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 138907-70-7
ethyl 5-amino-1-(3-fluorophenyl)-1H-pyrazole-4-carboxylate

: 1613395-78-0
C₂₂H₂₂ClF₄N₅O₄S

Guidance literature:: Multi-step reaction with 7 steps

1.1: diiodomethane; isopentyl nitrite / acetonitrile / 1 h / 20 - 50 °C

2.1: lithium hydroxide monohydrate; water / methanol; tetrahydrofuran

3.1: triethylamine; diphenyl phosphoryl azide / 20 - 60 °C / Molecular sieve

4.1: palladium diacetate; tricyclohexylphosphine; potassium phosphate / toluene; water / 7 h / 100 - 110 °C / Inert atmosphere

4.2: 100 °C

5.1: hydrogenchloride / 1,4-dioxane / 4 h / 20 °C

6.1: trimethylaluminum / 1,2-dichloro-ethane; toluene / 4 h / 20 °C

7.1: triethylamine / dichloromethane / 2 h / 20 °C

With hydrogenchloride; potassium phosphate; lithium hydroxide monohydrate; diiodomethane; diphenyl phosphoryl azide; water; trimethylaluminum; palladium diacetate; triethylamine; tricyclohexylphosphine; isopentyl nitrite; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; 1,2-dichloro-ethane; toluene; acetonitrile; 4.1: |Suzuki Coupling;

Reference yield:

: 1613395-67-7
ethyl 5-iodo-1-(3-fluorophenyl)-1H-pyrazole-4-carboxylate

: 1613395-78-0
C₂₂H₂₂ClF₄N₅O₄S

Guidance literature:: Multi-step reaction with 6 steps

1.1: lithium hydroxide monohydrate; water / methanol; tetrahydrofuran

2.1: triethylamine; diphenyl phosphoryl azide / 20 - 60 °C / Molecular sieve

3.1: palladium diacetate; tricyclohexylphosphine; potassium phosphate / toluene; water / 7 h / 100 - 110 °C / Inert atmosphere

3.2: 100 °C

4.1: hydrogenchloride / 1,4-dioxane / 4 h / 20 °C

5.1: trimethylaluminum / 1,2-dichloro-ethane; toluene / 4 h / 20 °C

6.1: triethylamine / dichloromethane / 2 h / 20 °C

With hydrogenchloride; potassium phosphate; lithium hydroxide monohydrate; diphenyl phosphoryl azide; water; trimethylaluminum; palladium diacetate; triethylamine; tricyclohexylphosphine; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; 1,2-dichloro-ethane; toluene; 3.1: |Suzuki Coupling;

Reference yield:

: 1567126-75-3
5-iodo-1-(3-fluorophenyl)-1H-pyrazole-4-carboxylic acid

: 1613395-78-0
C₂₂H₂₂ClF₄N₅O₄S

Guidance literature:: Multi-step reaction with 5 steps

1.1: triethylamine; diphenyl phosphoryl azide / 20 - 60 °C / Molecular sieve

2.1: palladium diacetate; tricyclohexylphosphine; potassium phosphate / toluene; water / 7 h / 100 - 110 °C / Inert atmosphere

2.2: 100 °C

3.1: hydrogenchloride / 1,4-dioxane / 4 h / 20 °C

4.1: trimethylaluminum / 1,2-dichloro-ethane; toluene / 4 h / 20 °C

5.1: triethylamine / dichloromethane / 2 h / 20 °C

With hydrogenchloride; potassium phosphate; diphenyl phosphoryl azide; trimethylaluminum; palladium diacetate; triethylamine; tricyclohexylphosphine; In 1,4-dioxane; dichloromethane; water; 1,2-dichloro-ethane; toluene; 2.1: |Suzuki Coupling;