C₃₁H₄₉O₇ISi

Base Information

Chemical Name:C₃₁H₄₉O₇ISi
CAS No.:250577-84-5
Molecular Formula:C₃₁H₄₉IO₇Si
Molecular Weight:688.716
Hs Code.:

C<sub>31</sub>H<sub>49</sub>O<sub>7</sub>ISi

Synonyms:C₃₁H₄₉O₇ISi

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₁H₄₉O₇ISi

Chemical Property:

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Technology Process of C₃₁H₄₉O₇ISi

There total 20 articles about C₃₁H₄₉O₇ISi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 250577-77-6
C₃₁SiH₄₀O₄

: 250577-84-5
C₃₁H₄₉O₇ISi

Guidance literature:: Multi-step reaction with 13 steps

1.1: 75 percent / H₂ / Pd/C / ethanol / 24 h / 2068.65 Torr

2.1: dimethyl sulfoxide; oxalyl chloride; ethyldiisopropylamine / CH₂Cl₂ / 0.92 h / -78 - 20 °C

3.1: 3.39 g / toluene / 1 h / 70 °C

4.1: sodium hexamethyldisilazide / tetrahydrofuran / 0 - 20 °C

4.2: 82 percent / tetrahydrofuran / 0.58 h / -78 - 20 °C

5.1: 73 percent / diisobutylaluminum hydride / CH₂Cl₂; hexane / -78 - 0 °C

6.1: triethylamine / CH₂Cl₂ / 0 - 20 °C

7.1: 3.53 g / sodium iodide / acetone / 2 h / Heating

8.1: 98 percent / benzene / 14 h / Heating

9.1: sodium hexamethyldisilazide / tetrahydrofuran / 1 h / -78 °C

9.2: 78 percent / tetrahydrofuran / -78 - 20 °C

10.1: 90 mg / benzene; CH₂Cl₂ / 120 h / 20 °C

11.1: 99 percent / diisobutylaluminum hydride / CH₂Cl₂; toluene / 0.08 h / -78 °C

12.1: triethylamine / CH₂Cl₂ / 0 - 20 °C

13.1: 126 mg / sodium iodide / acetone / 1 h / Heating

With oxalyl dichloride; hydrogen; sodium hexamethyldisilazane; diisobutylaluminium hydride; dimethyl sulfoxide; triethylamine; N-ethyl-N,N-diisopropylamine; sodium iodide; palladium on activated charcoal; In tetrahydrofuran; ethanol; hexane; dichloromethane; acetone; toluene; benzene; 2.1: Swern oxidation / 3.1: Wittig olefination / 4.2: Wittig olefination / 10.1: Wittig olefination;
DOI:10.1021/ol990281j

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 250577-84-5
C₃₁H₄₉O₇ISi

Guidance literature:: Multi-step reaction with 14 steps

1.1: 98 percent / imidazole / dimethylformamide / 0.5 h / 20 °C

2.1: 75 percent / H₂ / Pd/C / ethanol / 24 h / 2068.65 Torr

3.1: dimethyl sulfoxide; oxalyl chloride; ethyldiisopropylamine / CH₂Cl₂ / 0.92 h / -78 - 20 °C

4.1: 3.39 g / toluene / 1 h / 70 °C

5.1: sodium hexamethyldisilazide / tetrahydrofuran / 0 - 20 °C

5.2: 82 percent / tetrahydrofuran / 0.58 h / -78 - 20 °C

6.1: 73 percent / diisobutylaluminum hydride / CH₂Cl₂; hexane / -78 - 0 °C

7.1: triethylamine / CH₂Cl₂ / 0 - 20 °C

8.1: 3.53 g / sodium iodide / acetone / 2 h / Heating

9.1: 98 percent / benzene / 14 h / Heating

10.1: sodium hexamethyldisilazide / tetrahydrofuran / 1 h / -78 °C

10.2: 78 percent / tetrahydrofuran / -78 - 20 °C

11.1: 90 mg / benzene; CH₂Cl₂ / 120 h / 20 °C

12.1: 99 percent / diisobutylaluminum hydride / CH₂Cl₂; toluene / 0.08 h / -78 °C

13.1: triethylamine / CH₂Cl₂ / 0 - 20 °C

14.1: 126 mg / sodium iodide / acetone / 1 h / Heating

With 1H-imidazole; oxalyl dichloride; hydrogen; sodium hexamethyldisilazane; diisobutylaluminium hydride; dimethyl sulfoxide; triethylamine; N-ethyl-N,N-diisopropylamine; sodium iodide; palladium on activated charcoal; In tetrahydrofuran; ethanol; hexane; dichloromethane; N,N-dimethyl-formamide; acetone; toluene; benzene; 3.1: Swern oxidation / 4.1: Wittig olefination / 5.2: Wittig olefination / 11.1: Wittig olefination;
DOI:10.1021/ol990281j