Triphenyl(methanol-13C)

Base Information

Chemical Name:Triphenyl(methanol-13C)
CAS No.:3881-15-0
Molecular Formula:C₁₉H₁₆O
Molecular Weight:261.324
Hs Code.:
European Community (EC) Number:693-066-0
DSSTox Substance ID:DTXSID90583630
Wikidata:Q82475226
Mol file:3881-15-0.mol

Synonyms:Triphenyl(methanol-13C);3881-15-0;triphenyl(113C)methanol;Triphenyl(~13~C)methanol;SCHEMBL1332873;DTXSID90583630;Triphenyl(methanol-13C), 99 atom % 13C

Suppliers and Price of Triphenyl(methanol-13C)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
TRIPHENYL(METHANOL-13C) 95.00%
250MG
$ 763.42

Total 2 raw suppliers

Chemical Property of Triphenyl(methanol-13C)

Chemical Property:

Melting Point:163-165 °C(lit.)
Refractive Index:1.621
PSA：20.23000
Density:1.13g/cm³
LogP:3.97080
XLogP3:3.7
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:3
Exact Mass:261.123469965
Heavy Atom Count:20
Complexity:235

Purity/Quality:

98%min ^*data from raw suppliers

TRIPHENYL(METHANOL-13C) 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s): Xi
Hazard Codes:Xi
Statements: 38
Safety Statements: 22-24/25

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)C(C2=CC=CC=C2)(C3=CC=CC=C3)O
Isomeric SMILES:C1=CC=C(C=C1)[13C](C2=CC=CC=C2)(C3=CC=CC=C3)O

Technology Process of Triphenyl(methanol-13C)

There total 4 articles about Triphenyl(methanol-13C) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 52947-05-4
[α-13C]benzoyl chloride

: phenylmagnesium bromide

: 3881-15-0
<13C>-Triphenylmethanol

Guidance literature:: In diethyl ether; 1.) 0 deg C, 30 min; 2.) r.t., 2 h;
DOI:10.1002/hlca.19830660128

Reference yield: 55.0%

: 1111-72-4
carbon dioxide

: 591-51-5
phenyllithium

: 3880-99-7
1-(13C)benzoic acid

: 32488-48-5
benzophenone

: 3881-15-0
<13C>-Triphenylmethanol

Guidance literature:: In diethyl ether; hexane; at 20 ℃; for 0.333333h; Title compound not separated from byproducts;
DOI:10.1055/s-2001-18702

Reference yield:

: 3880-99-7
1-(13C)benzoic acid

: 3881-15-0
<13C>-Triphenylmethanol

Guidance literature:: Multi-step reaction with 2 steps

1: 99.9 percent / PCl₅ / 1.5 h / 60 °C

2: 90 percent / diethyl ether / 1.) 0 deg C, 30 min; 2.) r.t., 2 h

With phosphorus pentachloride; In diethyl ether;
DOI:10.1002/hlca.19830660128