α-methyl-α-furfuryl alcohol

Base Information

• Chemical Name: α-methyl-α-furfuryl alcohol
• CAS No.: 81830-82-2
• Molecular Formula: C₁₈H₁₆O₄S
• Molecular Weight: 328.389
• Mol file: 81830-82-2.mol

Synonyms:α-methyl-α-furfuryl alcohol

Chemical Property of α-methyl-α-furfuryl alcohol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of α-methyl-α-furfuryl alcohol

There total 1 articles about α-methyl-α-furfuryl alcohol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

furan (110-00-9) + 4'-(phenylsulfonyl)acetophenone (65085-83-8) → α-methyl-α-furfuryl alcohol (81830-82-2)

Guidance literature:

Multistep reaction;

DOI:10.1021/jo00137a005

Reference yield:

α-methyl-α-furfuryl alcohol (81830-82-2) → 6-hydroxy-2--2-methyl-2H-pyran-3(6H)-one (102285-69-8)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In chloroform; at 10 - 15 ℃; for 3h; Yield given;

DOI:10.1021/jo00137a005

Reference yield:

α-methyl-α-furfuryl alcohol (81830-82-2) → 6-methoxy-2--2-methyl-2H-pyran-3(6H)-one (81830-85-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 83percent m-chloroperbenzoic acid (MCPBA) / CHCl₃ / 3 h / 10 - 15 °C

2: 70.8 percent / Ag₂O / acetone

With 3-chloro-benzenecarboperoxoic acid; silver(l) oxide; In chloroform; acetone;

DOI:10.1021/jo00137a005

upstream raw materials:

furan

4'-(phenylsulfonyl)acetophenone

Downstream raw materials:

6-hydroxy-2--2-methyl-2H-pyran-3(6H)-one

2--2-methyl-2H-pyran-3,5-dione

2--2-methyl-6-<<(methylamino)carbonyl>oxy>-3-oxo-3,6-dihydro-2H-pyran

5-(4-Benzenesulfonyl-phenyl)-1,5-dimethyl-dihydro-pyrano[3,2-d]oxazole-2,6-dione