Technology Process of C23H40O5Si
There total 5 articles about C23H40O5Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
methanol; barium hydroxide octahydrate;
for 1h;
DOI:10.1021/jo3026077
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: copper(l) iodide / diethyl ether / 0.25 h / 0 °C / Inert atmosphere
1.2: 2 h / -50 °C / Inert atmosphere
2.1: water; acetic acid / tetrahydrofuran / 2.17 h / 0 - 5 °C
3.1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran; toluene / 2.17 h / 0 - 20 °C
4.1: methanol; barium hydroxide octahydrate / 1 h
With
methanol; copper(l) iodide; barium hydroxide octahydrate; water; acetic acid; triphenylphosphine; diethylazodicarboxylate;
In
tetrahydrofuran; diethyl ether; toluene;
3.1: |Mitsunobu Displacement;
DOI:10.1021/jo3026077
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: n-butyllithium / tetrahydrofuran; hexane / 0.33 h / 0 °C / Inert atmosphere
1.2: 0.33 h / 0 °C / Inert atmosphere
2.1: copper(l) iodide / diethyl ether / 0.25 h / 0 °C / Inert atmosphere
2.2: 2 h / -50 °C / Inert atmosphere
3.1: water; acetic acid / tetrahydrofuran / 2.17 h / 0 - 5 °C
4.1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran; toluene / 2.17 h / 0 - 20 °C
5.1: methanol; barium hydroxide octahydrate / 1 h
With
methanol; copper(l) iodide; n-butyllithium; barium hydroxide octahydrate; water; acetic acid; triphenylphosphine; diethylazodicarboxylate;
In
tetrahydrofuran; diethyl ether; hexane; toluene;
4.1: |Mitsunobu Displacement;
DOI:10.1021/jo3026077
