2-(naphthalen-1-yl)-1-phenyldiazene oxide

Base Information

• Chemical Name: 2-(naphthalen-1-yl)-1-phenyldiazene oxide
• CAS No.: 29558-69-8
• Molecular Formula: C₁₆H₁₂N₂O
• Molecular Weight: 248.284

Synonyms:2-(naphthalen-1-yl)-1-phenyldiazene oxide

Chemical Property of 2-(naphthalen-1-yl)-1-phenyldiazene oxide

Chemical Property:

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Technology Process of 2-(naphthalen-1-yl)-1-phenyldiazene oxide

There total 4 articles about 2-(naphthalen-1-yl)-1-phenyldiazene oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

1-amino-naphthalene (134-32-7) + Nitrosobenzene (586-96-9) → (Z)-2-(naphthalene-1-yl)-1-phenyldiazene 1-oxide (29558-69-8)

Guidance literature:

With pyridine; oxygen; copper(l) chloride; In toluene; at 65 ℃; for 24h; Schlenk technique;

DOI:10.1002/adsc.202001526

Reference yield:

nitrobenzene (98-95-3,26969-40-4) + C10H7N(2-)*2Br(1-)*2Mg(2+) → 2-(naphthalen-1-yl)-1-phenyldiazene oxide (29558-69-8)

Guidance literature:

In tetrahydrofuran; at 55 ℃; for 3h;

DOI:10.1246/bcsj.56.203

Reference yield:

Perbenzoic acid (93-59-4) + 1-phenylazonaphthalene (2653-70-5) → 2-(naphthalen-1-yl)-1-phenyldiazene oxide (29558-69-8)

Guidance literature:

With benzene;

DOI:10.1039/jr9530002147

upstream raw materials:

Perbenzoic acid

1-phenylazonaphthalene

nitrobenzene

1-amino-naphthalene

Downstream raw materials:

Sudan I

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