(3S)-3-<(tert-butoxycarbonyl)amino>-N-(4-chlorophenethyl)-2-hydroxy-6-<<<(tert-butoxycarbonyl)imino><<(4-methoxy-2,3,6-trimethylphenyl)sulfonyl>amino>methyl>amino>hexanamide

Base Information

Chemical Name:(3S)-3-<(tert-butoxycarbonyl)amino>-N-(4-chlorophenethyl)-2-hydroxy-6-<<<(tert-butoxycarbonyl)imino><<(4-methoxy-2,3,6-trimethylphenyl)sulfonyl>amino>methyl>amino>hexanamide
CAS No.:226985-38-2
Molecular Formula:C₃₅H₅₂ClN₅O₉S
Molecular Weight:754.345
Hs Code.:

(3S)-3-<(tert-butoxycarbonyl)amino>-N-(4-chlorophenethyl)-2-hydroxy-6-<<<(tert-butoxycarbonyl)imino><<(4-methoxy-2,3,6-trimethylphenyl)sulfonyl>amino>methyl>amino>hexanamide

Synonyms:(3S)-3-<(tert-butoxycarbonyl)amino>-N-(4-chlorophenethyl)-2-hydroxy-6-<<<(tert-butoxycarbonyl)imino><<(4-methoxy-2,3,6-trimethylphenyl)sulfonyl>amino>methyl>amino>hexanamide

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Chemical Property of (3S)-3-<(tert-butoxycarbonyl)amino>-N-(4-chlorophenethyl)-2-hydroxy-6-<<<(tert-butoxycarbonyl)imino><<(4-methoxy-2,3,6-trimethylphenyl)sulfonyl>amino>methyl>amino>hexanamide

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Technology Process of (3S)-3-<(tert-butoxycarbonyl)amino>-N-(4-chlorophenethyl)-2-hydroxy-6-<<<(tert-butoxycarbonyl)imino><<(4-methoxy-2,3,6-trimethylphenyl)sulfonyl>amino>methyl>amino>hexanamide

There total 1 articles about (3S)-3-<(tert-butoxycarbonyl)amino>-N-(4-chlorophenethyl)-2-hydroxy-6-<<<(tert-butoxycarbonyl)imino><<(4-methoxy-2,3,6-trimethylphenyl)sulfonyl>amino>methyl>amino>hexanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 156-41-2
4-chlorophenylethylamine

: 142801-56-7
(S)-3-tert-Butoxycarbonylamino-6-{[[(Z)-tert-butoxycarbonylimino]-(4-methoxy-2,3,6-trimethyl-benzenesulfonylamino)-methyl]-amino}-2-hydroxy-hexanoic acid

: 226985-38-2
(3S)-3-<(tert-butoxycarbonyl)amino>-N-(4-chlorophenethyl)-2-hydroxy-6-<<<(tert-butoxycarbonyl)imino><<(4-methoxy-2,3,6-trimethylphenyl)sulfonyl>amino>methyl>amino>hexanamide

Guidance literature:: With benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; Ambient temperature;
DOI:10.1021/jm980354p

Reference yield:

: 226985-38-2
(3S)-3-<(tert-butoxycarbonyl)amino>-N-(4-chlorophenethyl)-2-hydroxy-6-<<<(tert-butoxycarbonyl)imino><<(4-methoxy-2,3,6-trimethylphenyl)sulfonyl>amino>methyl>amino>hexanamide

: 203453-56-9
(3S)-3-amino-N-(4-chlorophenethyl)-2-hydroxy-6-<(imino<<(4-methoxy-2,3,6-trimethylphenyl)sulfonyl>amino>methyl)amino>hexanamide

Guidance literature:: With toluene-4-sulfonic acid; In tetrahydrofuran; Ambient temperature;
DOI:10.1021/jm980354p

Reference yield:

: 226985-38-2
(3S)-3-<(tert-butoxycarbonyl)amino>-N-(4-chlorophenethyl)-2-hydroxy-6-<<<(tert-butoxycarbonyl)imino><<(4-methoxy-2,3,6-trimethylphenyl)sulfonyl>amino>methyl>amino>hexanamide

: (1R,7R)-7-Amino-7-benzyl-8-oxo-hexahydro-pyrazolo[1,2-a]pyridazine-1-carboxylic acid {(S)-1-[2-(4-chloro-phenyl)-ethylaminooxalyl]-4-guanidino-butyl}-amide

Guidance literature:: Multi-step reaction with 4 steps

1: p-toluenesulfonic acid monohydrate / tetrahydrofuran / Ambient temperature

2: 1.) HOBt hydrate, diisopropylethylamine, EDC / 1.) THF, RT, 10 min, 2.) THF, RT, 15 h

3: Dess-Martin periodinane / CH₂Cl₂ / 6 h / Ambient temperature

4: 95 percent aq. trifluoroacetic acid, thioanisole / 30 h / Ambient temperature

With methyl-phenyl-thioether; benzotriazol-1-ol; Dess-Martin periodane; toluene-4-sulfonic acid; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jm980354p