diethyl (1S)-1-{N-benzylaminosulfate}-2-[(2-phenylethyl)amino]ethylphosphonate

Base Information

Chemical Name:diethyl (1S)-1-{N-benzylaminosulfate}-2-[(2-phenylethyl)amino]ethylphosphonate
CAS No.:854265-84-2
Molecular Formula:C₂₁H₃₁N₂O₆PS
Molecular Weight:470.527
Hs Code.:

Synonyms:diethyl (1S)-1-{N-benzylaminosulfate}-2-[(2-phenylethyl)amino]ethylphosphonate

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Chemical Property of diethyl (1S)-1-{N-benzylaminosulfate}-2-[(2-phenylethyl)amino]ethylphosphonate

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Technology Process of diethyl (1S)-1-{N-benzylaminosulfate}-2-[(2-phenylethyl)amino]ethylphosphonate

There total 5 articles about diethyl (1S)-1-{N-benzylaminosulfate}-2-[(2-phenylethyl)amino]ethylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 854265-73-9
diethyl ((4S)-3-benzyl-1,2,3-oxathiazolidine 2,2-dioxide)-4-phosphonate

: 64-04-0
phenethylamine

: 854265-84-2
diethyl (1S)-1-{N-benzylaminosulfate}-2-[(2-phenylethyl)amino]ethylphosphonate

Guidance literature:: In tetrahydrofuran;
DOI:10.1016/j.tetasy.2005.02.014

Reference yield:

: 854265-75-1
diethyl (1S)-(1-(N-benzylamino))-2-hydroxyethyl phosphonate

: 854265-84-2
diethyl (1S)-1-{N-benzylaminosulfate}-2-[(2-phenylethyl)amino]ethylphosphonate

Guidance literature:: Multi-step reaction with 3 steps

1: imidazole; Et₃N; thionyl chloride / CH₂Cl₂; CHCl₃ / 0.5 h / 0 °C

2: 63 percent / RuCl₃; NaIO₄ / acetonitrile; H₂O / 0 - 20 °C

3: 50 percent / tetrahydrofuran

With 1H-imidazole; ruthenium trichloride; sodium periodate; thionyl chloride; triethylamine; In tetrahydrofuran; dichloromethane; chloroform; water; acetonitrile;
DOI:10.1016/j.tetasy.2005.02.014

Reference yield:

: 854265-77-3
((S)-3-Benzyl-2-oxo-2λ⁴-[1,2,3]oxathiazolidin-4-yl)-phosphonic acid diethyl ester

: 854265-84-2
diethyl (1S)-1-{N-benzylaminosulfate}-2-[(2-phenylethyl)amino]ethylphosphonate

Guidance literature:: Multi-step reaction with 2 steps

1: 63 percent / RuCl₃; NaIO₄ / acetonitrile; H₂O / 0 - 20 °C

2: 50 percent / tetrahydrofuran

With ruthenium trichloride; sodium periodate; In tetrahydrofuran; water; acetonitrile;
DOI:10.1016/j.tetasy.2005.02.014