diethyl ((4S)-3-benzyl-1,2,3-oxathiazolidine 2,2-dioxide)-4-phosphonate

Base Information

Chemical Name:diethyl ((4S)-3-benzyl-1,2,3-oxathiazolidine 2,2-dioxide)-4-phosphonate
CAS No.:854265-73-9
Molecular Formula:C₁₃H₂₀NO₆PS
Molecular Weight:349.345
Hs Code.:

Synonyms:diethyl ((4S)-3-benzyl-1,2,3-oxathiazolidine 2,2-dioxide)-4-phosphonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of diethyl ((4S)-3-benzyl-1,2,3-oxathiazolidine 2,2-dioxide)-4-phosphonate

Chemical Property:

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Technology Process of diethyl ((4S)-3-benzyl-1,2,3-oxathiazolidine 2,2-dioxide)-4-phosphonate

There total 4 articles about diethyl ((4S)-3-benzyl-1,2,3-oxathiazolidine 2,2-dioxide)-4-phosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 854265-77-3
((S)-3-Benzyl-2-oxo-2λ⁴-[1,2,3]oxathiazolidin-4-yl)-phosphonic acid diethyl ester

: 854265-73-9
diethyl ((4S)-3-benzyl-1,2,3-oxathiazolidine 2,2-dioxide)-4-phosphonate

Guidance literature:: With ruthenium trichloride; sodium periodate; In water; acetonitrile; at 0 - 20 ℃;
DOI:10.1016/j.tetasy.2005.02.014

Reference yield:

: 854265-75-1
diethyl (1S)-(1-(N-benzylamino))-2-hydroxyethyl phosphonate

: 854265-73-9
diethyl ((4S)-3-benzyl-1,2,3-oxathiazolidine 2,2-dioxide)-4-phosphonate

Guidance literature:: Multi-step reaction with 2 steps

1: imidazole; Et₃N; thionyl chloride / CH₂Cl₂; CHCl₃ / 0.5 h / 0 °C

2: 63 percent / RuCl₃; NaIO₄ / acetonitrile; H₂O / 0 - 20 °C

With 1H-imidazole; ruthenium trichloride; sodium periodate; thionyl chloride; triethylamine; In dichloromethane; chloroform; water; acetonitrile;
DOI:10.1016/j.tetasy.2005.02.014

Reference yield:

: 100-52-7
benzaldehyde

: 854265-73-9
diethyl ((4S)-3-benzyl-1,2,3-oxathiazolidine 2,2-dioxide)-4-phosphonate

Guidance literature:: Multi-step reaction with 3 steps

1: 64 percent / acetic acid; NaCNBH₃ / ethanol / 18 h

2: imidazole; Et₃N; thionyl chloride / CH₂Cl₂; CHCl₃ / 0.5 h / 0 °C

3: 63 percent / RuCl₃; NaIO₄ / acetonitrile; H₂O / 0 - 20 °C

With 1H-imidazole; ruthenium trichloride; sodium periodate; thionyl chloride; sodium cyanoborohydride; acetic acid; triethylamine; In ethanol; dichloromethane; chloroform; water; acetonitrile;
DOI:10.1016/j.tetasy.2005.02.014