p-tolyl 4-O-tert-butoxycarbonyl-3-azido-2,3,6-trideoxy-1-thio-α-L-lyxopyranoside

Base Information

Chemical Name:p-tolyl 4-O-tert-butoxycarbonyl-3-azido-2,3,6-trideoxy-1-thio-α-L-lyxopyranoside
CAS No.:1083237-00-6
Molecular Formula:C₁₈H₂₅N₃O₄S
Molecular Weight:379.48
Hs Code.:

Synonyms:p-tolyl 4-O-tert-butoxycarbonyl-3-azido-2,3,6-trideoxy-1-thio-α-L-lyxopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of p-tolyl 4-O-tert-butoxycarbonyl-3-azido-2,3,6-trideoxy-1-thio-α-L-lyxopyranoside

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Technology Process of p-tolyl 4-O-tert-butoxycarbonyl-3-azido-2,3,6-trideoxy-1-thio-α-L-lyxopyranoside

There total 1 articles about p-tolyl 4-O-tert-butoxycarbonyl-3-azido-2,3,6-trideoxy-1-thio-α-L-lyxopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 936330-82-4
p-tolyl 3-azido-2,3,6-trideoxy-1-thio-α-L-arabino-hexopyranoside

: 24424-99-5
di-tert-butyl dicarbonate

: 1083237-00-6
p-tolyl 4-O-tert-butoxycarbonyl-3-azido-2,3,6-trideoxy-1-thio-α-L-lyxopyranoside

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 20 ℃;
DOI:10.1021/jo801630m

Reference yield:

: 1083237-00-6
p-tolyl 4-O-tert-butoxycarbonyl-3-azido-2,3,6-trideoxy-1-thio-α-L-lyxopyranoside

: 108-93-0
cyclohexanol

: cyclohexyl 4-O-tert-butoxycarbonyl-3-azido-2,3,6-trideoxy-1-L-lyxopyranoside

: 1083237-02-8
cyclohexyl 4-O-tert-butoxycarbonyl-3-azido-2,3,6-trideoxy-1-β-L-lyxopyranoside

Guidance literature:: p-tolyl 4-O-tert-butoxycarbonyl-3-azido-2,3,6-trideoxy-1-thio-α-L-lyxopyranoside; With 1-(phenylsulfonyl)piperidine; 2,4,5-tri-tert-butylpyrimidine; In dichloromethane; at -60 ℃; for 0.166667h; Molecular sieve; Inert atmosphere;

With trifluoromethylsulfonic anhydride; In dichloromethane; Inert atmosphere; Cooling;

cyclohexanol; In dichloromethane; at -60 ℃; for 2h; optical yield given as %de;
DOI:10.1021/jo801630m