2,11-bis(diphenylphosphinomethyl)benzophenanthrene

Base Information

• Chemical Name: 2,11-bis(diphenylphosphinomethyl)benzophenanthrene
• CAS No.: 61892-31-7
• Molecular Formula: C₄₄H₃₄P₂
• Molecular Weight: 624.701

Synonyms:2,11-bis(diphenylphosphinomethyl)benzophenanthrene

Chemical Property of 2,11-bis(diphenylphosphinomethyl)benzophenanthrene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,11-bis(diphenylphosphinomethyl)benzophenanthrene

There total 4 articles about 2,11-bis(diphenylphosphinomethyl)benzophenanthrene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,11-bis(bromomethyl)benzophenanthrene (61892-30-6) + diphenylphosphane (829-85-6) → 2,11-bis(diphenylphosphinomethyl)benzophenanthrene (61892-31-7)

Guidance literature:

Multistep reaction; (i) nBuLi, hexane, (ii) /BRN= 2535167/, THF;

DOI:10.1002/hlca.19760590806

Reference yield:

2,2-bis-(4-methyl-phenethyl)-oxirane (61892-27-1) → 2,11-bis(diphenylphosphinomethyl)benzophenanthrene (61892-31-7)

Guidance literature:

Multi-step reaction with 4 steps

1: BF₃-Et₂O / benzene

2: DDQ / benzene

3: NBS, (PhCO)2O₂ / CCl₄ / Heating

4: (i) nBuLi, hexane, (ii) /BRN= 2535167/, THF

With N-Bromosuccinimide; boron trifluoride diethyl etherate; 2,3-dicyano-5,6-dichloro-p-benzoquinone; dibenzoyl peroxide; In tetrachloromethane; benzene;

DOI:10.1002/hlca.19760590806

Reference yield:

2,11-Dimethyl-5,6,6a,7,8,12b-hexahydro-benzo[c]phenanthrene (61892-28-2) → 2,11-bis(diphenylphosphinomethyl)benzophenanthrene (61892-31-7)

Guidance literature:

Multi-step reaction with 3 steps

1: DDQ / benzene

2: NBS, (PhCO)2O₂ / CCl₄ / Heating

3: (i) nBuLi, hexane, (ii) /BRN= 2535167/, THF

With N-Bromosuccinimide; 2,3-dicyano-5,6-dichloro-p-benzoquinone; dibenzoyl peroxide; In tetrachloromethane; benzene;

DOI:10.1002/hlca.19760590806

upstream raw materials:

2,11-bis(bromomethyl)benzophenanthrene

diphenylphosphane

2,2-bis-(4-methyl-phenethyl)-oxirane

2,11-dimethylbenzophenanthrene

Downstream raw materials:

trans-{PtHCl⁽¹⁾}

{Pt(ethylene)(2,11-bis(diphenylphosphinomethyl)benzo{c}phenanthrene)}

{Pt(C₂H₄)2(C₆H₅)2PCH₂C₁₈H₁₀CH₂P(C₆H₅)2Pt(C₂H₄)2}

{Pt(H₃CO₂CCCCO₂CH₃)(2,11-bis(diphenylphosphinomethyl)benzo{c}phenanthrene)}

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 61892-31-7 2,11-bis(diphenylphosphinomethyl)benzophenanthrene

Send

Send

Metric Ton KG G Pound L ML

Send

Send