tert-butyl-2-(4-(2,3-dichlorophenyl)piperazin-1-yl)-2-oxoethylcarbamate

Base Information

Chemical Name:tert-butyl-2-(4-(2,3-dichlorophenyl)piperazin-1-yl)-2-oxoethylcarbamate
CAS No.:1470068-47-3
Molecular Formula:C₁₇H₂₃Cl₂N₃O₃
Molecular Weight:388.294
Hs Code.:

Synonyms:tert-butyl-2-(4-(2,3-dichlorophenyl)piperazin-1-yl)-2-oxoethylcarbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tert-butyl-2-(4-(2,3-dichlorophenyl)piperazin-1-yl)-2-oxoethylcarbamate

Chemical Property:

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Technology Process of tert-butyl-2-(4-(2,3-dichlorophenyl)piperazin-1-yl)-2-oxoethylcarbamate

There total 1 articles about tert-butyl-2-(4-(2,3-dichlorophenyl)piperazin-1-yl)-2-oxoethylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 119532-26-2,864512-47-0
1-(2,3-dichlorophenyl)-piperazine hydrochloride

: 4530-20-5
BOC-glycine

: 1470068-47-3
tert-butyl-2-(4-(2,3-dichlorophenyl)piperazin-1-yl)-2-oxoethylcarbamate

Guidance literature:: BOC-glycine; With 4-methyl-morpholine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In acetonitrile; at 0 ℃; for 0.166667h;

1-(2,3-dichlorophenyl)-piperazine hydrochloride; With 4-methyl-morpholine; benzotriazol-1-ol; In N,N-dimethyl-formamide; acetonitrile; at 20 ℃; pH=8;
DOI:10.2174/0929866511320080005

Reference yield:

: 1470068-47-3
tert-butyl-2-(4-(2,3-dichlorophenyl)piperazin-1-yl)-2-oxoethylcarbamate

: 76-05-1
trifluoroacetic acid

: C₁₂H₁₅Cl₂N₃O*C₂HF₃O₂

Guidance literature:: at 20 ℃; for 0.75h;
DOI:10.2174/0929866511320080005

Reference yield:

: 1470068-47-3
tert-butyl-2-(4-(2,3-dichlorophenyl)piperazin-1-yl)-2-oxoethylcarbamate

: 1470068-61-1
C₁₉H₁₉BrCl₂N₄OS

Guidance literature:: Multi-step reaction with 2 steps

1: 0.75 h / 20 °C

2: 4-methyl-morpholine / N,N-dimethyl-formamide / 8 h / 0 - 20 °C

With 4-methyl-morpholine; In N,N-dimethyl-formamide;
DOI:10.2174/0929866511320080005