2-((4-chlorophenyl)amino)-N-methyl-N-(methylsulfonyl)-2-phenylacetamide

Base Information

• Chemical Name: 2-((4-chlorophenyl)amino)-N-methyl-N-(methylsulfonyl)-2-phenylacetamide
• CAS No.: 1333483-28-5
• Molecular Formula: C₁₆H₁₇ClN₂O₃S
• Molecular Weight: 352.842
• Mol file: 1333483-28-5.mol

Synonyms:2-((4-chlorophenyl)amino)-N-methyl-N-(methylsulfonyl)-2-phenylacetamide

Chemical Property of 2-((4-chlorophenyl)amino)-N-methyl-N-(methylsulfonyl)-2-phenylacetamide

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of 2-((4-chlorophenyl)amino)-N-methyl-N-(methylsulfonyl)-2-phenylacetamide

There total 1 articles about 2-((4-chlorophenyl)amino)-N-methyl-N-(methylsulfonyl)-2-phenylacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

N-(4-chlorophenyl)-α-phenylnitrone (19865-58-8,32213-73-3) + N-methyll-N-(phenylethylnyl)methanesulfonamide (1333483-14-9) → 2-((4-chlorophenyl)amino)-N-methyl-N-(methylsulfonyl)-2-phenylacetamide (1333483-28-5)

Guidance literature:

With silver hexafluoroantimonate; 2-(di-tert-butylphosphino)-1,1'-biphenylgold(I) chloride; In water; 1,2-dichloro-ethane; at 25 ℃; for 10h; Inert atmosphere;

DOI:10.1021/ja208150d

Reference yield:

2-((4-chlorophenyl)amino)-N-methyl-N-(methylsulfonyl)-2-phenylacetamide (1333483-28-5) → 2-((4-chlorophenyl)amino)-2-phenylethanol

Guidance literature:

With sodium tetrahydroborate; In tetrahydrofuran; water; 1,2-dichloro-ethane; at 25 ℃; for 0.333333h; Inert atmosphere;

DOI:10.1021/ja208150d

upstream raw materials:

N-(4-chlorophenyl)-α-phenylnitrone

N-methyll-N-(phenylethylnyl)methanesulfonamide