Benzenesulfinic acid benzhydrylideneamide

Base Information

• Chemical Name: Benzenesulfinic acid benzhydrylideneamide
• CAS No.: 75168-64-8
• Molecular Formula: C₁₉H₁₅NOS
• Molecular Weight: 305.4
• Mol file: 75168-64-8.mol

Synonyms:Benzenesulfinic acid benzhydrylideneamide

Chemical Property of Benzenesulfinic acid benzhydrylideneamide

Chemical Property:

Purity/Quality:

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Technology Process of Benzenesulfinic acid benzhydrylideneamide

There total 5 articles about Benzenesulfinic acid benzhydrylideneamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

phenyl(diphenylmethyleneamino)chlorosulfonium chloride → Benzenesulfinic acid benzhydrylideneamide (75168-64-8)

Guidance literature:

With water; triethylamine; In diethyl ether; at 20 ℃; for 1h;

Reference yield: 82.5%

benzenesulphinyl chloride (4972-29-6) + Benzophenone imine (1013-88-3) → Benzenesulfinic acid benzhydrylideneamide (75168-64-8)

Guidance literature:

With triethylamine; In diethyl ether; at 20 ℃; for 2h;

Reference yield:

Benzophenone imine (1013-88-3) → Benzenesulfinic acid benzhydrylideneamide (75168-64-8)

Guidance literature:

Multi-step reaction with 3 steps

1: 87.5 percent / triethylamine / diethyl ether / 2 h / 20 °C

2: 82 percent / chlorine / CCl₄ / 24 h / 20 °C

3: 90 percent / triethylamine, water / diethyl ether / 1 h / 20 °C

With water; chlorine; triethylamine; In tetrachloromethane; diethyl ether;

upstream raw materials:

benzenesulphinyl chloride

Benzophenone imine

N-(diphenylmethylene)-S-phenylthiohydroxylamine

benzenesulfenyl chloride