diphenyl-[2-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]phosphine borane

Base Information

Chemical Name:diphenyl-[2-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]phosphine borane
CAS No.:1417911-71-7
Molecular Formula:C₂₄H₂₉B₂O₂P
Molecular Weight:402.089
Hs Code.:

Synonyms:diphenyl-[2-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]phosphine borane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of diphenyl-[2-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]phosphine borane

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Technology Process of diphenyl-[2-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]phosphine borane

There total 8 articles about diphenyl-[2-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]phosphine borane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 14044-65-6
borane-THF

: 1250258-94-6
[2-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)phenyl]diphenylphosphine

: 1417911-71-7
diphenyl-[2-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]phosphine borane

Guidance literature:: In tetrahydrofuran; at 20 ℃; for 3h; Inert atmosphere;
DOI:10.1002/anie.201813278

Reference yield: 86.0%

: 14044-65-6
borane-THF

: 603-35-0
triphenylphosphine

: 73183-34-3
bis(pinacol)diborane

: 1417911-71-7
diphenyl-[2-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]phosphine borane

: phenylbis(2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)phosphane borane

Guidance literature:: triphenylphosphine; bis(pinacol)diborane; With chlorobis(cyclooctene)rhodium(I) dimer; benzene-1,2-diol; 4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane; In toluene; at 110 ℃; for 12h; Inert atmosphere; Schlenk technique; Sealed tube;

borane-THF; In tetrahydrofuran; at 0 - 20 ℃; for 2h; Inert atmosphere; Schlenk technique; Sealed tube;
DOI:10.1002/anie.201813452

Reference yield: 51.0%

: 61676-62-8
2-Isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 1257322-37-4
(2-bromophenyl)-diphenylphosphine borane

: 1417911-71-7
diphenyl-[2-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]phosphine borane

Guidance literature:: (2-bromophenyl)-diphenylphosphine borane; With n-butyllithium; In tetrahydrofuran; at -78 ℃; for 1h; Inert atmosphere;

2-Isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane; In tetrahydrofuran; at -78 - 20 ℃; for 20.5h;