Technology Process of C25H27N7
There total 14 articles about C25H27N7 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
trifluoroacetic acid;
In
dichloromethane;
at 20 ℃;
for 10h;
DOI:10.1021/jm401836p
- Guidance literature:
-
With
trifluoroacetic acid;
In
dichloromethane;
at 20 ℃;
for 10h;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 1.17 h / 20 °C
2.1: ammonium acetate / xylenes / 2 h / 140 °C
2.2: Alkaline conditions
3.1: potassium acetate / tetrakis(triphenylphosphine) palladium(0) / 1,4-dioxane / 16.5 h / 80 °C
4.1: sodium hydrogencarbonate / tetrakis(triphenylphosphine) palladium(0) / 1,2-dimethoxyethane; water / 24 h / 80 °C
5.1: trifluoroacetic acid / dichloromethane / 10 h / 20 °C
With
ammonium acetate; potassium acetate; sodium hydrogencarbonate; N-ethyl-N,N-diisopropylamine; HATU; trifluoroacetic acid;
tetrakis(triphenylphosphine) palladium(0);
In
1,4-dioxane; 1,2-dimethoxyethane; dichloromethane; water; N,N-dimethyl-formamide; xylenes;