(2R,3S,4R)-2-(4-methoxybenzyloxy)-4-methyl-3-(triethylsilyloxy)hex-5-ene

Base Information

• Chemical Name: (2R,3S,4R)-2-(4-methoxybenzyloxy)-4-methyl-3-(triethylsilyloxy)hex-5-ene
• CAS No.: 1234550-43-6
• Molecular Formula: C₂₁H₃₆O₃Si
• Molecular Weight: 364.601

Synonyms:(2R,3S,4R)-2-(4-methoxybenzyloxy)-4-methyl-3-(triethylsilyloxy)hex-5-ene

Chemical Property of (2R,3S,4R)-2-(4-methoxybenzyloxy)-4-methyl-3-(triethylsilyloxy)hex-5-ene

Chemical Property:

Purity/Quality:

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Technology Process of (2R,3S,4R)-2-(4-methoxybenzyloxy)-4-methyl-3-(triethylsilyloxy)hex-5-ene

There total 1 articles about (2R,3S,4R)-2-(4-methoxybenzyloxy)-4-methyl-3-(triethylsilyloxy)hex-5-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

(2S,3S,4R)-4-(4-methoxybenzyloxy)-2-methyl-3-(triethylsilyloxy)pentanal (1234550-42-5) + Methyltriphenylphosphonium bromide (1779-49-3) → (2R,3S,4R)-2-(4-methoxybenzyloxy)-4-methyl-3-(triethylsilyloxy)hex-5-ene (1234550-43-6)

Guidance literature:

Methyltriphenylphosphonium bromide; With n-butyllithium; In tetrahydrofuran; hexane; at 0 ℃;

(2S,3S,4R)-4-(4-methoxybenzyloxy)-2-methyl-3-(triethylsilyloxy)pentanal; In tetrahydrofuran; hexane; at -78 - 20 ℃;

DOI:10.1016/j.tet.2010.04.039

Reference yield: 98.0%

(2R,3S,4R)-2-(4-methoxybenzyloxy)-4-methyl-3-(triethylsilyloxy)hex-5-ene (1234550-43-6) → (2R,3S,4R)-2-(4-methoxybenzyloxy)-4-methylhex-5-en-3-ol (1234550-38-9)

Guidance literature:

With hydrogen fluoride; water; In acetonitrile; at 20 ℃; for 3h;

DOI:10.1016/j.tet.2010.04.039

upstream raw materials:

(2S,3S,4R)-4-(4-methoxybenzyloxy)-2-methyl-3-(triethylsilyloxy)pentanal

Methyltriphenylphosphonium bromide

Downstream raw materials:

(2R,3S,4R)-2-(4-methoxybenzyloxy)-4-methylhex-5-en-3-ol

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