2-(3-aminophenyl)ethanesulfonic acid benzenesulfonylamide

Base Information

Chemical Name:2-(3-aminophenyl)ethanesulfonic acid benzenesulfonylamide
CAS No.:838826-29-2
Molecular Formula:C₁₄H₁₆N₂O₄S₂
Molecular Weight:340.424
Hs Code.:

Synonyms:2-(3-aminophenyl)ethanesulfonic acid benzenesulfonylamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(3-aminophenyl)ethanesulfonic acid benzenesulfonylamide

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Technology Process of 2-(3-aminophenyl)ethanesulfonic acid benzenesulfonylamide

There total 5 articles about 2-(3-aminophenyl)ethanesulfonic acid benzenesulfonylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 402508-80-9
2-(3-nitrophenyl)ethanesulfonic acid benzenesulfonylamide

: 838826-29-2
2-(3-aminophenyl)ethanesulfonic acid benzenesulfonylamide

Guidance literature:: With hydrogen; 10percent Pd/C; In methanol; at 20 ℃; for 4h; under 760.051 Torr;
DOI:10.1021/jm0101500

Reference yield:

: 98-09-9
benzenesulfonyl chloride

: 838826-29-2
2-(3-aminophenyl)ethanesulfonic acid benzenesulfonylamide

Guidance literature:: Multi-step reaction with 2 steps

1: 54 percent / Et₃N / acetonitrile / 4 h / Heating

2: 99 percent / H₂ / 10percent Pd/C / methanol / 4 h / 20 °C / 760.05 Torr

With hydrogen; triethylamine; 10percent Pd/C; In methanol; acetonitrile;
DOI:10.1021/jm0101500

Reference yield:

: 402508-78-5
2-(3-nitrophenyl)ethanesulfonic acid

: 838826-29-2
2-(3-aminophenyl)ethanesulfonic acid benzenesulfonylamide

Guidance literature:: Multi-step reaction with 4 steps

1: SOCl₂ / dimethylformamide / 17 h / Heating

2: NH₃ / dioxane / 5 h / 20 °C

3: 54 percent / Et₃N / acetonitrile / 4 h / Heating

4: 99 percent / H₂ / 10percent Pd/C / methanol / 4 h / 20 °C / 760.05 Torr

With thionyl chloride; ammonia; hydrogen; triethylamine; 10percent Pd/C; In 1,4-dioxane; methanol; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jm0101500