1-[3-({[tert-butyl(dimethyl)silyl]oxy}methyl)phenyl]cyclopropyl acetate

Base Information

Chemical Name:1-[3-({[tert-butyl(dimethyl)silyl]oxy}methyl)phenyl]cyclopropyl acetate
CAS No.:1346690-10-5
Molecular Formula:C₁₈H₂₈O₃Si
Molecular Weight:320.504
Hs Code.:

Synonyms:1-[3-({[tert-butyl(dimethyl)silyl]oxy}methyl)phenyl]cyclopropyl acetate

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Chemical Property of 1-[3-({[tert-butyl(dimethyl)silyl]oxy}methyl)phenyl]cyclopropyl acetate

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Technology Process of 1-[3-({[tert-butyl(dimethyl)silyl]oxy}methyl)phenyl]cyclopropyl acetate

There total 1 articles about 1-[3-({[tert-butyl(dimethyl)silyl]oxy}methyl)phenyl]cyclopropyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1346690-09-2
1-[3-({[tert-butyl(dimethyl)silyl]oxy}methyl)phenyl]cyclopropanol

: 75-36-5
acetyl chloride

: 1346690-10-5
1-[3-({[tert-butyl(dimethyl)silyl]oxy}methyl)phenyl]cyclopropyl acetate

Guidance literature:: With ethylmagnesium chloride; In tetrahydrofuran; at 20 ℃; for 0.0833333h;

Reference yield:

: 1346690-10-5
1-[3-({[tert-butyl(dimethyl)silyl]oxy}methyl)phenyl]cyclopropyl acetate

: 1346690-65-0
1-[3-(hydroxymethyl)phenyl]cyclopropyl acetate

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 0.5h;

Reference yield:

: 1346690-10-5
1-[3-({[tert-butyl(dimethyl)silyl]oxy}methyl)phenyl]cyclopropyl acetate

: 1346690-11-6
1-(3-{[(methylsulphonyl)oxy]methyl}phenyl)cyclopropyl acetate

Guidance literature:: Multi-step reaction with 2 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.5 h / 20 °C

2: triethylamine / tetrahydrofuran / 0.17 h / 0 - 20 °C

With tetrabutyl ammonium fluoride; triethylamine; In tetrahydrofuran;