1--2,4-cyclohexadiene

Base Information

Chemical Name:1--2,4-cyclohexadiene
CAS No.:106093-52-1
Molecular Formula:C₁₁H₁₄O₅
Molecular Weight:226.229
Hs Code.:

1-<bis(methoxycarbonyl)methoxy>-2,4-cyclohexadiene

Synonyms:1--2,4-cyclohexadiene

Suppliers and Price of 1--2,4-cyclohexadiene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1--2,4-cyclohexadiene

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Technology Process of 1--2,4-cyclohexadiene

There total 2 articles about 1--2,4-cyclohexadiene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.5%

: 6773-29-1
dimethyl diazomalonate

: 66542-65-2,127943-86-6
cyclohexa-2,4-dien-1-ol

: 106093-52-1
1--2,4-cyclohexadiene

Guidance literature:: With dirhodium tetraacetate; In benzene; at 65 ℃; for 2h;
DOI:10.1021/ja00238a029

Reference yield:

: 108-59-8
malonic acid dimethyl ester

: 106093-52-1
1--2,4-cyclohexadiene

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / p-TsN₃, Et₃N / benzene / 15 h / Ambient temperature

2: 36.5 percent / rhodium acetate dimer / benzene / 2 h / 65 °C

With dirhodium tetraacetate; 4-toluenesulfonyl azide; triethylamine; In benzene;
DOI:10.1021/ja00238a029