3-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-N-(diphenoxyphosphoryl)-L-serine tetradecanamide

Base Information

Chemical Name:3-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-N-(diphenoxyphosphoryl)-L-serine tetradecanamide
CAS No.:350689-32-6
Molecular Formula:C₄₃H₆₃N₂O₁₄P
Molecular Weight:862.952
Hs Code.:

Synonyms:3-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-N-(diphenoxyphosphoryl)-L-serine tetradecanamide

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Chemical Property of 3-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-N-(diphenoxyphosphoryl)-L-serine tetradecanamide

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Technology Process of 3-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-N-(diphenoxyphosphoryl)-L-serine tetradecanamide

There total 4 articles about 3-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-N-(diphenoxyphosphoryl)-L-serine tetradecanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 2524-64-3
chlorophosphoric acid diphenyl ester

: 171191-27-8
3-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-L-serine tetradecylamide

: 350689-32-6
3-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-N-(diphenoxyphosphoryl)-L-serine tetradecanamide

Guidance literature:: With pyridine; at 0 ℃; for 2h;
DOI:10.1021/jm0011124

Reference yield:

: 2016-42-4
tetradecylamine

: 350689-32-6
3-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-N-(diphenoxyphosphoryl)-L-serine tetradecanamide

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / HOBt; EDC / CH₂Cl₂ / 0 - 20 °C

2: 76 percent / morpholine / dimethylformamide / 4 h / 20 °C

3: 80 percent / pyridine / 2 h / 0 °C

With morpholine; pyridine; benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm0011124

Reference yield:

: 96383-44-7
N^α-(9-fluoroenylmethoxycarbonyl)-3-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-L-serine

: 350689-32-6
3-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-N-(diphenoxyphosphoryl)-L-serine tetradecanamide

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / HOBt; EDC / CH₂Cl₂ / 0 - 20 °C

2: 76 percent / morpholine / dimethylformamide / 4 h / 20 °C

3: 80 percent / pyridine / 2 h / 0 °C

With morpholine; pyridine; benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm0011124