4-O-benzoyl-2-fluoro-2,3,6-trideoxy-3-(trifluoroacetamido)-α-L-galactopyranosyl bromide

Base Information

Chemical Name:4-O-benzoyl-2-fluoro-2,3,6-trideoxy-3-(trifluoroacetamido)-α-L-galactopyranosyl bromide
CAS No.:107384-12-3
Molecular Formula:C₁₅H₁₄BrF₄NO₄
Molecular Weight:428.178
Hs Code.:

Synonyms:4-O-benzoyl-2-fluoro-2,3,6-trideoxy-3-(trifluoroacetamido)-α-L-galactopyranosyl bromide

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Chemical Property of 4-O-benzoyl-2-fluoro-2,3,6-trideoxy-3-(trifluoroacetamido)-α-L-galactopyranosyl bromide

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Technology Process of 4-O-benzoyl-2-fluoro-2,3,6-trideoxy-3-(trifluoroacetamido)-α-L-galactopyranosyl bromide

There total 4 articles about 4-O-benzoyl-2-fluoro-2,3,6-trideoxy-3-(trifluoroacetamido)-α-L-galactopyranosyl bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: acetyl 4-O-benzoyl-2-fluoro-2,3,6-trideoxy-3-(trifluoroacetamido)-β-L-galactopyranoside

: 107384-12-3
4-O-benzoyl-2-fluoro-2,3,6-trideoxy-3-(trifluoroacetamido)-α-L-galactopyranosyl bromide

Guidance literature:: With hydrogen bromide; In acetic acid; for 1h; Ambient temperature;
DOI:10.1021/jo00224a052

Reference yield:

: 99018-08-3
benzyl 3-azido-4,6-O-benzylidene-2,3-dideoxy-2-fluoro-α-D-altropyranoside

: 107384-12-3
4-O-benzoyl-2-fluoro-2,3,6-trideoxy-3-(trifluoroacetamido)-α-L-galactopyranosyl bromide

Guidance literature:: Multi-step reaction with 4 steps

1: 96 percent / pyridine / 48 h / Ambient temperature

2: 91 percent / H₂ / 10percent Pd/C / methanol / 760 Torr

3: 96 percent / sodium acetate / 0.5 h / Heating

4: 86 percent / 33percent HBr / acetic acid / 1 h / Ambient temperature

With pyridine; hydrogen bromide; hydrogen; sodium acetate; palladium on activated charcoal; In methanol; acetic acid;
DOI:10.1021/jo00224a052

Reference yield:

: 99018-16-3
benzyl 4-O-benzoyl-2-fluoro-2,3,6-trideoxy-3-(trifluoroacetamido)-β-L-galactopyranoside

: 107384-12-3
4-O-benzoyl-2-fluoro-2,3,6-trideoxy-3-(trifluoroacetamido)-α-L-galactopyranosyl bromide

Guidance literature:: Multi-step reaction with 3 steps

1: 91 percent / H₂ / 10percent Pd/C / methanol / 760 Torr

2: 96 percent / sodium acetate / 0.5 h / Heating

3: 86 percent / 33percent HBr / acetic acid / 1 h / Ambient temperature

With hydrogen bromide; hydrogen; sodium acetate; palladium on activated charcoal; In methanol; acetic acid;
DOI:10.1021/jo00224a052