benzyl 4-O-benzoyl-2-fluoro-2,3,6-trideoxy-3-(trifluoroacetamido)-β-L-galactopyranoside

Base Information

Chemical Name:benzyl 4-O-benzoyl-2-fluoro-2,3,6-trideoxy-3-(trifluoroacetamido)-β-L-galactopyranoside
CAS No.:99018-16-3
Molecular Formula:C₂₂H₂₁F₄NO₅
Molecular Weight:455.406
Hs Code.:

Synonyms:benzyl 4-O-benzoyl-2-fluoro-2,3,6-trideoxy-3-(trifluoroacetamido)-β-L-galactopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzyl 4-O-benzoyl-2-fluoro-2,3,6-trideoxy-3-(trifluoroacetamido)-β-L-galactopyranoside

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Technology Process of benzyl 4-O-benzoyl-2-fluoro-2,3,6-trideoxy-3-(trifluoroacetamido)-β-L-galactopyranoside

There total 1 articles about benzyl 4-O-benzoyl-2-fluoro-2,3,6-trideoxy-3-(trifluoroacetamido)-β-L-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 98-88-4
benzoyl chloride

: 99018-08-3
benzyl 3-azido-4,6-O-benzylidene-2,3-dideoxy-2-fluoro-α-D-altropyranoside

: 99018-16-3
benzyl 4-O-benzoyl-2-fluoro-2,3,6-trideoxy-3-(trifluoroacetamido)-β-L-galactopyranoside

Guidance literature:: With pyridine; for 48h; Ambient temperature;
DOI:10.1021/jo00224a052

Reference yield: 91.0%

: 99018-16-3
benzyl 4-O-benzoyl-2-fluoro-2,3,6-trideoxy-3-(trifluoroacetamido)-β-L-galactopyranoside

: 99018-17-4
4-O-benzoyl-2-fluoro-2,3,6-trideoxy-3-(trifluoroacetamido)-L-galactopyranoside

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; under 760 Torr;
DOI:10.1021/jo00224a052

Reference yield:

: 99018-16-3
benzyl 4-O-benzoyl-2-fluoro-2,3,6-trideoxy-3-(trifluoroacetamido)-β-L-galactopyranoside

: 107384-12-3
4-O-benzoyl-2-fluoro-2,3,6-trideoxy-3-(trifluoroacetamido)-α-L-galactopyranosyl bromide

Guidance literature:: Multi-step reaction with 3 steps

1: 91 percent / H₂ / 10percent Pd/C / methanol / 760 Torr

2: 96 percent / sodium acetate / 0.5 h / Heating

3: 86 percent / 33percent HBr / acetic acid / 1 h / Ambient temperature

With hydrogen bromide; hydrogen; sodium acetate; palladium on activated charcoal; In methanol; acetic acid;
DOI:10.1021/jo00224a052