o-methoxycarbonylphenyl 2,3-di-O-benzyl-4,6-O-benzylidene-1-thio-β-D-galactopyranoside

Base Information

Chemical Name:o-methoxycarbonylphenyl 2,3-di-O-benzyl-4,6-O-benzylidene-1-thio-β-D-galactopyranoside
CAS No.:1101186-12-2
Molecular Formula:C₃₅H₃₄O₇S
Molecular Weight:598.717
Hs Code.:

Synonyms:o-methoxycarbonylphenyl 2,3-di-O-benzyl-4,6-O-benzylidene-1-thio-β-D-galactopyranoside

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Chemical Property of o-methoxycarbonylphenyl 2,3-di-O-benzyl-4,6-O-benzylidene-1-thio-β-D-galactopyranoside

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Technology Process of o-methoxycarbonylphenyl 2,3-di-O-benzyl-4,6-O-benzylidene-1-thio-β-D-galactopyranoside

There total 1 articles about o-methoxycarbonylphenyl 2,3-di-O-benzyl-4,6-O-benzylidene-1-thio-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1101186-11-1
C₂₁H₂₂O₇S

: 100-39-0
benzyl bromide

: 1101186-12-2
o-methoxycarbonylphenyl 2,3-di-O-benzyl-4,6-O-benzylidene-1-thio-β-D-galactopyranoside

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 18h; Inert atmosphere;
DOI:10.1016/j.carres.2008.09.028

Reference yield: 60.0%

: 1101186-12-2
o-methoxycarbonylphenyl 2,3-di-O-benzyl-4,6-O-benzylidene-1-thio-β-D-galactopyranoside

: 190779-65-8
2,3-di-O-(4-methoxybenzyl)-sn-glycerol

: 1101186-18-8
3-O-(2',3'-di-O-benzyl-4',6'-O-benzylidene-β-D-galactopyranosyl)-1,2-di-O-(4-methoxybenzyl)-sn-glycerol

: 1101186-26-8
C₄₆H₅₀O₁₀

Guidance literature:: o-methoxycarbonylphenyl 2,3-di-O-benzyl-4,6-O-benzylidene-1-thio-β-D-galactopyranoside; 2,3-di-O-(4-methoxybenzyl)-sn-glycerol; In dichloromethane; acetonitrile; at 20 ℃; for 3h; Molecular sieve; Inert atmosphere;

With N-iodo-succinimide; In dichloromethane; acetonitrile; at -40 - 20 ℃; Inert atmosphere;

With trifluorormethanesulfonic acid; In dichloromethane; acetonitrile; at -40 ℃; for 0.5h; Inert atmosphere;
DOI:10.1016/j.carres.2008.09.028

Reference yield:

: 1101186-12-2
o-methoxycarbonylphenyl 2,3-di-O-benzyl-4,6-O-benzylidene-1-thio-β-D-galactopyranoside

: 1114560-40-5
3-O-(2',3',4'-tri-O-benzyl-β-D-galactopyranosyl)-1,2-di-O-(4-methoxybenzyl)-sn-glycerol

: 1114560-42-7
3-O-[(2'',3''-di-O-benzyl-4'',6''-O-benzylidene-β-D-galactopyranosyl)-(1->6)-(2',3',4'-tri-O-benzyl-β-D-galactopyranosyl)]-1,2-di-O-(4-methoxybenzyl)-sn-glycerol

Guidance literature:: o-methoxycarbonylphenyl 2,3-di-O-benzyl-4,6-O-benzylidene-1-thio-β-D-galactopyranoside; 3-O-(2',3',4'-tri-O-benzyl-β-D-galactopyranosyl)-1,2-di-O-(4-methoxybenzyl)-sn-glycerol; In dichloromethane; acetonitrile; at 20 ℃; for 3h; Molecular sieve; Inert atmosphere;

With N-iodo-succinimide; In dichloromethane; acetonitrile; at -40 - 20 ℃; Inert atmosphere;

With trifluorormethanesulfonic acid; In dichloromethane; acetonitrile; at -40 ℃; for 0.5h; Inert atmosphere;
DOI:10.1016/j.carres.2008.09.028