ethyl 2-ethoxycarbonylmethylthio-3-<4-(2-methyl-2-phenylpropoxy)phenyl>propionate

Base Information

Chemical Name:ethyl 2-ethoxycarbonylmethylthio-3-<4-(2-methyl-2-phenylpropoxy)phenyl>propionate
CAS No.:85021-76-7
Molecular Formula:C₂₅H₃₂O₅S
Molecular Weight:444.592
Hs Code.:

Synonyms:ethyl 2-ethoxycarbonylmethylthio-3-<4-(2-methyl-2-phenylpropoxy)phenyl>propionate

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Chemical Property of ethyl 2-ethoxycarbonylmethylthio-3-<4-(2-methyl-2-phenylpropoxy)phenyl>propionate

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Technology Process of ethyl 2-ethoxycarbonylmethylthio-3-<4-(2-methyl-2-phenylpropoxy)phenyl>propionate

There total 1 articles about ethyl 2-ethoxycarbonylmethylthio-3-<4-(2-methyl-2-phenylpropoxy)phenyl>propionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.4%

: 62516-91-0,74401-63-1
ethyl 2-chloro-3-[4-(2,2-dimethyl-2-phenylethyloxy)phenyl]propionate

: 623-51-8
ethyl 2-sulfanylacetate

: 85021-76-7
ethyl 2-ethoxycarbonylmethylthio-3-<4-(2-methyl-2-phenylpropoxy)phenyl>propionate

Guidance literature:: With sodium ethanolate; In ethanol; for 2h; Ambient temperature;
DOI:10.1248/cpb.30.3563

Reference yield:

: 85021-76-7
ethyl 2-ethoxycarbonylmethylthio-3-<4-(2-methyl-2-phenylpropoxy)phenyl>propionate

: 2-Carboxymethylsulfanyl-3-[4-(2-methyl-2-phenyl-propoxy)-phenyl]-propionic acid

Guidance literature:: With potassium hydroxide; In ethanol; for 10h; Heating;
DOI:10.1248/cpb.30.3563

Reference yield:

: 85021-76-7
ethyl 2-ethoxycarbonylmethylthio-3-<4-(2-methyl-2-phenylpropoxy)phenyl>propionate

: 85021-75-6
2-<4-(2-methyl-2-phenylpropoxy)benzyl>-perhydro-1,4-thiazine-3,5-dione

Guidance literature:: Multi-step reaction with 3 steps

1: 2N KOH / ethanol / 10 h / Heating

2: 1.) ethyl chloroformate, Et₃N, 2.) NH₃ / 1.) THF, 15 min, 2.) THF, EtOH, 5 deg C, 15 min

3: 13.4 percent / 1.5 h / 200 °C

With potassium hydroxide; ammonia; chloroformic acid ethyl ester; triethylamine; In ethanol;
DOI:10.1248/cpb.30.3563