methyl (E)-3-[2-(4-hydroxy-3,5-dimethoxyphenyl)-7-hydroxy-3-methoxycarbonyl-2,3-dihydro-1-benzofuran-5-yl]propen-2-enoate

Base Information

Chemical Name:methyl (E)-3-[2-(4-hydroxy-3,5-dimethoxyphenyl)-7-hydroxy-3-methoxycarbonyl-2,3-dihydro-1-benzofuran-5-yl]propen-2-enoate
CAS No.:1316855-24-9
Molecular Formula:C₂₂H₂₂O₉
Molecular Weight:430.411
Hs Code.:

Synonyms:methyl (E)-3-[2-(4-hydroxy-3,5-dimethoxyphenyl)-7-hydroxy-3-methoxycarbonyl-2,3-dihydro-1-benzofuran-5-yl]propen-2-enoate

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Chemical Property of methyl (E)-3-[2-(4-hydroxy-3,5-dimethoxyphenyl)-7-hydroxy-3-methoxycarbonyl-2,3-dihydro-1-benzofuran-5-yl]propen-2-enoate

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Technology Process of methyl (E)-3-[2-(4-hydroxy-3,5-dimethoxyphenyl)-7-hydroxy-3-methoxycarbonyl-2,3-dihydro-1-benzofuran-5-yl]propen-2-enoate

There total 6 articles about methyl (E)-3-[2-(4-hydroxy-3,5-dimethoxyphenyl)-7-hydroxy-3-methoxycarbonyl-2,3-dihydro-1-benzofuran-5-yl]propen-2-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 14.0%

: 3843-74-1,67667-67-8
methyl 3,4-dihydroxycinnamate

: 42041-51-0,67460-46-2,20733-94-2
4-hydroxy-3,5-dimethoxycinnamic acid methyl ester

: 1316855-26-1
methyl (E)-3-[2-(4-hydroxy-3,5-dimethoxyphenyl)-3-methoxycarbonyl-2,3-dihydro-1-4-benzodioxan-7-yl]propen-2-enoate

: 1316855-24-9
methyl (E)-3-[2-(4-hydroxy-3,5-dimethoxyphenyl)-7-hydroxy-3-methoxycarbonyl-2,3-dihydro-1-benzofuran-5-yl]propen-2-enoate

: 1316855-25-0
C₂₄H₂₈O₁₀

Guidance literature:: With dihydrogen peroxide; horseradish peroxidase; In 1,4-dioxane; water; at 0 ℃; for 4.75h; pH=3.5; Phosphate/citric acid buffer; Enzymatic reaction;
DOI:10.1016/j.tetlet.2011.05.072

Reference yield: 12.0%

: 3843-74-1,67667-67-8
methyl 3,4-dihydroxycinnamate

: 42041-51-0,67460-46-2,20733-94-2
4-hydroxy-3,5-dimethoxycinnamic acid methyl ester

: 1316855-24-9
methyl (E)-3-[2-(4-hydroxy-3,5-dimethoxyphenyl)-7-hydroxy-3-methoxycarbonyl-2,3-dihydro-1-benzofuran-5-yl]propen-2-enoate

: 1316855-25-0
C₂₄H₂₈O₁₀

Guidance literature:: With manganese(IV) oxide; dihydrogen peroxide; In 1,4-dioxane; water; at 0 ℃; for 4.75h; pH=3.5; Phosphate/citric acid buffer; Enzymatic reaction;
DOI:10.1016/j.tetlet.2011.05.072

Reference yield:

: 530-59-6,7362-37-0
sinapinic acid

: 1316855-24-9
methyl (E)-3-[2-(4-hydroxy-3,5-dimethoxyphenyl)-7-hydroxy-3-methoxycarbonyl-2,3-dihydro-1-benzofuran-5-yl]propen-2-enoate

: 1316855-25-0
C₂₄H₂₈O₁₀

Guidance literature:: Multi-step reaction with 2 steps

1: sulfuric acid

2: manganese(IV) oxide; dihydrogen peroxide / 1,4-dioxane; water / 4.75 h / 0 °C / pH 3.5 / Phosphate/citric acid buffer; Enzymatic reaction

With manganese(IV) oxide; sulfuric acid; dihydrogen peroxide; In 1,4-dioxane; water; 1: Fischer esterification;
DOI:10.1016/j.tetlet.2011.05.072