methyl 4-(3-nitrophenyl)-2-phenyl-6-trifluoromethyl-5-pyrimidinecarboxylate

Base Information

Chemical Name:methyl 4-(3-nitrophenyl)-2-phenyl-6-trifluoromethyl-5-pyrimidinecarboxylate
CAS No.:103311-97-3
Molecular Formula:C₂₀H₁₄F₃N₃O₄
Molecular Weight:417.344
Hs Code.:

Synonyms:methyl 4-(3-nitrophenyl)-2-phenyl-6-trifluoromethyl-5-pyrimidinecarboxylate

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Chemical Property of methyl 4-(3-nitrophenyl)-2-phenyl-6-trifluoromethyl-5-pyrimidinecarboxylate

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Technology Process of methyl 4-(3-nitrophenyl)-2-phenyl-6-trifluoromethyl-5-pyrimidinecarboxylate

There total 5 articles about methyl 4-(3-nitrophenyl)-2-phenyl-6-trifluoromethyl-5-pyrimidinecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 146379-74-0
4-(3-Nitro-phenyl)-2-phenyl-6-trifluoromethyl-1,4-dihydro-pyrimidine-5-carboxylic acid ethyl ester

: 103311-97-3
methyl 4-(3-nitrophenyl)-2-phenyl-6-trifluoromethyl-5-pyrimidinecarboxylate

Guidance literature:: With manganese(IV) oxide; In chloroform; for 2h; Yield given; Heating;
DOI:10.1248/cpb.40.2423

Reference yield:

: 1670-14-0
benzamidine monohydrochloride

: 103311-97-3
methyl 4-(3-nitrophenyl)-2-phenyl-6-trifluoromethyl-5-pyrimidinecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / butan-1-ol / 4 h / Heating

2: MnO₂ / CHCl₃ / 2 h / Heating

With manganese(IV) oxide; triethylamine; In chloroform; butan-1-ol;
DOI:10.1248/cpb.40.2423

Reference yield:

: 99-61-6
3-nitro-benzaldehyde

: 103311-97-3
methyl 4-(3-nitrophenyl)-2-phenyl-6-trifluoromethyl-5-pyrimidinecarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: piperidine, acetic acid / benzene / 1 h / Heating

2: Et₃N / butan-1-ol / 4 h / Heating

3: MnO₂ / CHCl₃ / 2 h / Heating

With piperidine; manganese(IV) oxide; acetic acid; triethylamine; In chloroform; butan-1-ol; benzene;
DOI:10.1248/cpb.40.2423