3-iodo-2-formylphenylboronic acid

Base Information

Chemical Name:3-iodo-2-formylphenylboronic acid
CAS No.:928048-13-9
Molecular Formula:C₇H₆BIO₃
Molecular Weight:275.838
Hs Code.:

Synonyms:3-iodo-2-formylphenylboronic acid

Suppliers and Price of 3-iodo-2-formylphenylboronic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 3-iodo-2-formylphenylboronic acid

Chemical Property:

Melting Point:80-83 °C
Boiling Point:433.3±55.0 °C(Predicted)
Density:1.96±0.1 g/cm3(Predicted)

Purity/Quality:: 95%-98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3-iodo-2-formylphenylboronic acid

There total 5 articles about 3-iodo-2-formylphenylboronic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 928048-16-2
2-formyl-3-(trimethylsilyl)phenylboronic acid

: 928048-13-9
3-iodo-2-formylphenylboronic acid

Guidance literature:: With Iodine monochloride; In chloroform; for 6h; Reflux; Inert atmosphere;
DOI:10.1016/j.jorganchem.2010.08.016

Reference yield: 85.0%

: 928048-16-2
2-formyl-3-(trimethylsilyl)phenylboronic acid

: 7790-99-0
Iodine monochloride

: 928048-13-9
3-iodo-2-formylphenylboronic acid

Guidance literature:: In chloroform; (Ar); stirring mixt. of boronic acid deriv., 1.1 equiv. of ICl and CHCl3at reflux for 6 h; concg., addn. of diethyl ether, addn. of aq. Na2S2O3, separating organicphase, evapn., filtration, washing with CHCl3, elem. anal.;
DOI:10.1016/j.jorganchem.2010.08.016

Reference yield:

: 67713-23-9
2,6-dibromobenzaldehyde

: 928048-13-9
3-iodo-2-formylphenylboronic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / H₂SO₄ / methanol / 1 h / Heating

With sulfuric acid; In methanol;
DOI:10.1039/b611195e