10-methyl-9-[(3-methylphenoxy)carbonyl]acridinium trifluoromethanesulfonate

Base Information

Chemical Name:10-methyl-9-[(3-methylphenoxy)carbonyl]acridinium trifluoromethanesulfonate
CAS No.:162704-51-0
Molecular Formula:CF₃O₃S*C₂₂H₁₈NO₂
Molecular Weight:477.461
Hs Code.:

Synonyms:10-methyl-9-[(3-methylphenoxy)carbonyl]acridinium trifluoromethanesulfonate

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Chemical Property of 10-methyl-9-[(3-methylphenoxy)carbonyl]acridinium trifluoromethanesulfonate

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Technology Process of 10-methyl-9-[(3-methylphenoxy)carbonyl]acridinium trifluoromethanesulfonate

There total 4 articles about 10-methyl-9-[(3-methylphenoxy)carbonyl]acridinium trifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 158749-58-7
3-methylphenyl acridine-9-carboxylate

: 333-27-7
methyl trifluoromethanesulfonate

: 162704-51-0
10-methyl-9-[(3-methylphenoxy)carbonyl]acridinium trifluoromethanesulfonate

Guidance literature:: In dichloromethane; at 20 ℃;
DOI:10.1016/j.saa.2007.10.045

Reference yield:

: 5336-90-3
acridine-9-carboxylic acid

: 162704-51-0
10-methyl-9-[(3-methylphenoxy)carbonyl]acridinium trifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: thionyl chloride / Reflux

2: dmap; triethylamine / dichloromethane / 20 °C

3: dichloromethane / 20 °C / Inert atmosphere

With dmap; thionyl chloride; triethylamine; In dichloromethane;
DOI:10.1021/jo1020882

Reference yield:

: 66074-67-7
9-acridinecarbonyl chloride

: 162704-51-0
10-methyl-9-[(3-methylphenoxy)carbonyl]acridinium trifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: dmap; triethylamine / dichloromethane / 20 °C

2: 2,6-di-tert-butyl-pyridine / dichloromethane / 20 °C

With dmap; 2,6-di-tert-butyl-pyridine; triethylamine; In dichloromethane;
DOI:10.1016/j.saa.2010.10.029