2,6-dimethyl-4-<2-(4-fluorophenyl)-2-methylethenyl>phenyl ethyl carbonate

Base Information

Chemical Name:2,6-dimethyl-4-<2-(4-fluorophenyl)-2-methylethenyl>phenyl ethyl carbonate
CAS No.:127063-67-6
Molecular Formula:C₂₀H₂₁FO₃
Molecular Weight:328.383
Hs Code.:

Synonyms:2,6-dimethyl-4-<2-(4-fluorophenyl)-2-methylethenyl>phenyl ethyl carbonate

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Chemical Property of 2,6-dimethyl-4-<2-(4-fluorophenyl)-2-methylethenyl>phenyl ethyl carbonate

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Technology Process of 2,6-dimethyl-4-<2-(4-fluorophenyl)-2-methylethenyl>phenyl ethyl carbonate

There total 3 articles about 2,6-dimethyl-4-<2-(4-fluorophenyl)-2-methylethenyl>phenyl ethyl carbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2233-18-3
4-hydroxy-3,5-dimethylbenzaldehyde

: 127063-67-6
2,6-dimethyl-4-<2-(4-fluorophenyl)-2-methylethenyl>phenyl ethyl carbonate

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / Et₃N / CH₂Cl₂ / 3.5 h / Heating

2: 1.) n-BuLi / 1.) ether, hexane, RT, 3 h, 2.) 24 h

With n-butyllithium; triethylamine; In dichloromethane;
DOI:10.1021/jm00169a010

Reference yield:

: 403-41-8
1-(4-Fluorophenyl)ethanol

: 127063-67-6
2,6-dimethyl-4-<2-(4-fluorophenyl)-2-methylethenyl>phenyl ethyl carbonate

Guidance literature:: Multi-step reaction with 2 steps

1: 91.5 percent / 30percent HBr / acetic acid / 21.5 h / 80 - 90 °C

2: 1.) n-BuLi / 1.) ether, hexane, RT, 3 h, 2.) 24 h

With n-butyllithium; hydrogen bromide; In acetic acid;
DOI:10.1021/jm00169a010

Reference yield:

: 403-42-9
1-(4-fluorophenyl)ethanone

: 127063-67-6
2,6-dimethyl-4-<2-(4-fluorophenyl)-2-methylethenyl>phenyl ethyl carbonate

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / NaBH₄ / propan-2-ol / 3.5 h / Ambient temperature

2: 91.5 percent / 30percent HBr / acetic acid / 21.5 h / 80 - 90 °C

3: 1.) n-BuLi / 1.) ether, hexane, RT, 3 h, 2.) 24 h

With sodium tetrahydroborate; n-butyllithium; hydrogen bromide; In acetic acid; isopropyl alcohol;
DOI:10.1021/jm00169a010