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((CH3)3C6H2)2Ge(F)NHC6H4CON(CH3)2

Base Information
  • Chemical Name:((CH3)3C6H2)2Ge(F)NHC6H4CON(CH3)2
  • CAS No.:146699-06-1
  • Molecular Formula:C27H33FGeN2O
  • Molecular Weight:493.16
  • Hs Code.:
((CH<sub>3</sub>)3C<sub>6</sub>H<sub>2</sub>)2Ge(F)NHC<sub>6</sub>H<sub>4</sub>CON(CH<sub>3</sub>)2

Synonyms:((CH3)3C6H2)2Ge(F)NHC6H4CON(CH3)2

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Chemical Property of ((CH3)3C6H2)2Ge(F)NHC6H4CON(CH3)2
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Technology Process of ((CH3)3C6H2)2Ge(F)NHC6H4CON(CH3)2

There total 1 articles about ((CH3)3C6H2)2Ge(F)NHC6H4CON(CH3)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
In benzene; byproducts: LiF; dropwise addn. of 2.15mmol Li-compound to a soln. of 2.15mmol Ge-compound in C6H6;; centrifugation, evapn. in vac., dissolving of residue in pentane (30°C), evapn.; elem. anal.;;
DOI:10.1021/om00028a008
Guidance literature:
In tetrahydrofuran; byproducts: LiF; under N2 or Ar; addn. LiMe2N/THF (freshly prepared from Me2NH and LiBu) to cooled (-40°C) soln. Ge-compd./THF, stirred 2 h; centrifuged (removal LiF), evapn., elem. anal.;
DOI:10.1016/0022-328X(93)83344-U
Guidance literature:
With tert.-butyl lithium; In not given; byproducts: LiF; method according to Riviere-Baudet et al., Organometallics, 12 (1993) p. 1003;
DOI:10.1016/0022-328X(93)83344-U
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