trans-1-amino-4-(2-{[2-bis(ethoxycarbonylmethylamino)ethyl]ethoxycarbonylmethylamino}acetylamino)cyclohexane

Base Information

Chemical Name:trans-1-amino-4-(2-{[2-bis(ethoxycarbonylmethylamino)ethyl]ethoxycarbonylmethylamino}acetylamino)cyclohexane
CAS No.:776297-90-6
Molecular Formula:C₂₂H₄₀N₄O₇
Molecular Weight:472.582
Hs Code.:

Synonyms:trans-1-amino-4-(2-{[2-bis(ethoxycarbonylmethylamino)ethyl]ethoxycarbonylmethylamino}acetylamino)cyclohexane

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Chemical Property of trans-1-amino-4-(2-{[2-bis(ethoxycarbonylmethylamino)ethyl]ethoxycarbonylmethylamino}acetylamino)cyclohexane

Chemical Property:

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Technology Process of trans-1-amino-4-(2-{[2-bis(ethoxycarbonylmethylamino)ethyl]ethoxycarbonylmethylamino}acetylamino)cyclohexane

There total 3 articles about trans-1-amino-4-(2-{[2-bis(ethoxycarbonylmethylamino)ethyl]ethoxycarbonylmethylamino}acetylamino)cyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 776297-89-3
trans-1-tert-butoxycarbonylamino-4-(2-{[2-bis(ethoxycarbonylmethylamino)ethyl]ethoxycarbonylmethylamino}acetylamino)cyclohexane

: 776297-90-6
trans-1-amino-4-(2-{[2-bis(ethoxycarbonylmethylamino)ethyl]ethoxycarbonylmethylamino}acetylamino)cyclohexane

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 18 ℃; for 0.5h;
DOI:10.1055/s-2004-829143

Reference yield:

: 177906-48-8
trans-N-Boc-1,4-cyclohexanediamine

: 776297-90-6
trans-1-amino-4-(2-{[2-bis(ethoxycarbonylmethylamino)ethyl]ethoxycarbonylmethylamino}acetylamino)cyclohexane

Guidance literature:: Multi-step reaction with 2 steps

1: 870 mg / tetrahydrofuran / 18 h / 4 °C

2: 81 percent / TFA / CH₂Cl₂ / 0.5 h / 18 °C

With trifluoroacetic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1055/s-2004-829143

Reference yield:

: [[2-(bis-ethoxycarbonylmethyl-amino)-ethyl]-(2-isobutoxycarbonyloxy-2-oxo-ethyl)-amino]-acetic acid ethyl ester

: 776297-90-6
trans-1-amino-4-(2-{[2-bis(ethoxycarbonylmethylamino)ethyl]ethoxycarbonylmethylamino}acetylamino)cyclohexane

Guidance literature:: Multi-step reaction with 2 steps

1: 870 mg / tetrahydrofuran / 18 h / 4 °C

2: 81 percent / TFA / CH₂Cl₂ / 0.5 h / 18 °C

With trifluoroacetic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1055/s-2004-829143