(E)-6-bromo-2-(2-(5-bromo-1-(phenylsulfonyl)-1H-indol-2-yl)vinyl)-1-(phenulsulfonyl)-1H-indole

Base Information

Chemical Name:(E)-6-bromo-2-(2-(5-bromo-1-(phenylsulfonyl)-1H-indol-2-yl)vinyl)-1-(phenulsulfonyl)-1H-indole
CAS No.:1572178-43-8
Molecular Formula:C₃₀H₂₀Br₂N₂O₄S₂
Molecular Weight:696.44
Hs Code.:

Synonyms:(E)-6-bromo-2-(2-(5-bromo-1-(phenylsulfonyl)-1H-indol-2-yl)vinyl)-1-(phenulsulfonyl)-1H-indole

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Chemical Property of (E)-6-bromo-2-(2-(5-bromo-1-(phenylsulfonyl)-1H-indol-2-yl)vinyl)-1-(phenulsulfonyl)-1H-indole

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Technology Process of (E)-6-bromo-2-(2-(5-bromo-1-(phenylsulfonyl)-1H-indol-2-yl)vinyl)-1-(phenulsulfonyl)-1H-indole

There total 6 articles about (E)-6-bromo-2-(2-(5-bromo-1-(phenylsulfonyl)-1H-indol-2-yl)vinyl)-1-(phenulsulfonyl)-1H-indole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

: 1572178-40-5
C₁₅H₁₁Br₂NO₂S

: 118757-11-2
1-Benzenesulfonyl-5-bromo-indole

: 1572178-43-8
(E)-6-bromo-2-(2-(5-bromo-1-(phenylsulfonyl)-1H-indol-2-yl)vinyl)-1-(phenulsulfonyl)-1H-indole

Guidance literature:: C₁₅H₁₁Br₂NO₂S; With triphenylphosphine; In dichloromethane; at 20 ℃; for 0.5h;

1-Benzenesulfonyl-5-bromo-indole; With 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; methanol; at 20 ℃; for 3h;

Reference yield:

: 1572178-41-6
C₃₃H₂₆BrNO₂PS⁽¹⁺⁾*Br^(1-)

: 1572178-42-7
C₁₅H₁₀BrNO₃S

: 1572178-43-8
(E)-6-bromo-2-(2-(5-bromo-1-(phenylsulfonyl)-1H-indol-2-yl)vinyl)-1-(phenulsulfonyl)-1H-indole

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In diethyl ether; at 20 ℃; for 3h;
DOI:10.1016/j.bmc.2014.01.020

Reference yield:

: 1572178-39-2
(6-bromo-1-(phenylsulfonyl)-1H-indol-2-yl)methanol

: 1572178-43-8
(E)-6-bromo-2-(2-(5-bromo-1-(phenylsulfonyl)-1H-indol-2-yl)vinyl)-1-(phenulsulfonyl)-1H-indole

Guidance literature:: Multi-step reaction with 3 steps

1: phosphorus tribromide / diethyl ether / 0.5 h / 0 - 20 °C

2: dichloromethane / 20 °C

3: 1,8-diazabicyclo[5.4.0]undec-7-ene / diethyl ether / 3 h / 20 °C

With phosphorus tribromide; 1,8-diazabicyclo[5.4.0]undec-7-ene; In diethyl ether; dichloromethane; 3: |Wittig Olefination;
DOI:10.1016/j.bmc.2014.01.020