(-)-(S)-2-phenyl-4-(triisopropylsilyl)-2-[((trimethylsilyl)ethynyl)]-but-3-ynal

Base Information

Chemical Name:(-)-(S)-2-phenyl-4-(triisopropylsilyl)-2-[((trimethylsilyl)ethynyl)]-but-3-ynal
CAS No.:1229626-59-8
Molecular Formula:C₂₄H₃₆OSi₂
Molecular Weight:396.72
Hs Code.:

Synonyms:(-)-(S)-2-phenyl-4-(triisopropylsilyl)-2-[((trimethylsilyl)ethynyl)]-but-3-ynal

Suppliers and Price of (-)-(S)-2-phenyl-4-(triisopropylsilyl)-2-[((trimethylsilyl)ethynyl)]-but-3-ynal

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (-)-(S)-2-phenyl-4-(triisopropylsilyl)-2-[((trimethylsilyl)ethynyl)]-but-3-ynal

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Technology Process of (-)-(S)-2-phenyl-4-(triisopropylsilyl)-2-[((trimethylsilyl)ethynyl)]-but-3-ynal

There total 1 articles about (-)-(S)-2-phenyl-4-(triisopropylsilyl)-2-[((trimethylsilyl)ethynyl)]-but-3-ynal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1229626-58-7
(-)-(S)-2-phenyl-4-(triisopropylsilyl)-2-[(trimethylsilyl)ethynyl]-3-butyn-1-ol

: 1229626-59-8
(-)-(S)-2-phenyl-4-(triisopropylsilyl)-2-[((trimethylsilyl)ethynyl)]-but-3-ynal

Guidance literature:: With Dess-Martin periodane; In dichloromethane; at 0 ℃; for 12h;
DOI:10.1002/ejoc.201000076

Reference yield: 83.0%

: 558-13-4
carbon tetrabromide

: 1229626-59-8
(-)-(S)-2-phenyl-4-(triisopropylsilyl)-2-[((trimethylsilyl)ethynyl)]-but-3-ynal

: 1229626-60-1
(-)-(R)-{5,5-dibromo-3-phenyl-3-[(triisopropylsilyl)ethynyl]-4-penten-1-yn-1-yl}(trimethyl)silane

Guidance literature:: carbon tetrabromide; With triphenylphosphine; In dichloromethane; at 0 ℃; for 0.25h;

(-)-(S)-2-phenyl-4-(triisopropylsilyl)-2-[((trimethylsilyl)ethynyl)]-but-3-ynal; In dichloromethane; at 0 ℃; for 3h;
DOI:10.1002/ejoc.201000076