N₂-[2-[1-[(4-chlorophenyl)methyl]-1H-imidazol-5-yl]ethyl]-N₁-cyclohexyl-1,2(R)-piperazinecarboxamide

Base Information

• Chemical Name: N₂-[2-[1-[(4-chlorophenyl)methyl]-1H-imidazol-5-yl]ethyl]-N₁-cyclohexyl-1,2(R)-piperazinecarboxamide
• CAS No.: 279238-48-1
• Molecular Formula: C₂₄H₃₃ClN₆O₂
• Molecular Weight: 473.018

Synonyms:N₂-[2-[1-[(4-chlorophenyl)methyl]-1H-imidazol-5-yl]ethyl]-N₁-cyclohexyl-1,2(R)-piperazinecarboxamide

Chemical Property of N₂-[2-[1-[(4-chlorophenyl)methyl]-1H-imidazol-5-yl]ethyl]-N₁-cyclohexyl-1,2(R)-piperazinecarboxamide

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Technology Process of N₂-[2-[1-[(4-chlorophenyl)methyl]-1H-imidazol-5-yl]ethyl]-N₁-cyclohexyl-1,2(R)-piperazinecarboxamide

There total 2 articles about N₂-[2-[1-[(4-chlorophenyl)methyl]-1H-imidazol-5-yl]ethyl]-N₁-cyclohexyl-1,2(R)-piperazinecarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N4-(1,1-dimethylethyloxycarbonyl)-N2-[2-[1-[(4-chlorophenyl)methyl]-1H-imidazol-5-yl]ethyl]-1,2(R)-piperazinecarboxamide (279237-41-1) + Cyclohexyl isocyanate (3173-53-3) → N2-[2-[1-[(4-chlorophenyl)methyl]-1H-imidazol-5-yl]ethyl]-N1-cyclohexyl-1,2(R)-piperazinecarboxamide (279238-48-1)

Guidance literature:

N₄-(1,1-dimethylethyloxycarbonyl)-N₂-[2-[1-[(4-chlorophenyl)methyl]-1H-imidazol-5-yl]ethyl]-1,2(R)-piperazinecarboxamide; Cyclohexyl isocyanate; In dichloromethane; at 20 ℃; for 0.5h;

With trifluoroacetic acid; In dichloromethane; at 20 ℃;

Reference yield:

→ N2-[2-[1-[(4-chlorophenyl)methyl]-1H-imidazol-5-yl]ethyl]-N1-cyclohexyl-1,2(R)-piperazinecarboxamide (279238-48-1)

Guidance literature:

Reference yield:

N2-[2-[1-[(4-chlorophenyl)methyl]-1H-imidazol-5-yl]ethyl]-N1-cyclohexyl-1,2(R)-piperazinecarboxamide (279238-48-1) + benzaldehyde (100-52-7) → N4-phenylmethyl-N2-[2-[1-[(4-chlorophenyl)methyl]-1H-imidazol-5-yl]ethyl]-N1-cyclohexyl-1,2(R)-piperazinedicarboxamide (281197-59-9)

Guidance literature:

With sodium tris(acetoxy)borohydride; In dichloromethane; acetic acid; at 0 - 20 ℃; for 12h;

upstream raw materials:

N₄-(1,1-dimethylethyloxycarbonyl)-N₂-[2-[1-[(4-chlorophenyl)methyl]-1H-imidazol-5-yl]ethyl]-1,2(R)-piperazinecarboxamide

Cyclohexyl isocyanate

Downstream raw materials:

N₄-phenylmethyl-N₂-[2-[1-[(4-chlorophenyl)methyl]-1H-imidazol-5-yl]ethyl]-N₁-cyclohexyl-1,2(R)-piperazinedicarboxamide

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