C₂₉H₂₉N₃O₂S

Base Information

• Chemical Name: C₂₉H₂₉N₃O₂S
• CAS No.: 1401113-29-8
• Molecular Formula: C₂₉H₂₉N₃O₂S
• Molecular Weight: 483.634
• Mol file: 1401113-29-8.mol

Synonyms:C₂₉H₂₉N₃O₂S

Chemical Property of C₂₉H₂₉N₃O₂S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₉H₂₉N₃O₂S

There total 3 articles about C₂₉H₂₉N₃O₂S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.3%

4-Nitrophenylacetonitrile (555-21-5,34512-13-5,174848-08-9) + 10-(2-ethylhexyl)-10H-3-phenothiazine carbaldehyde (501116-23-0) → C29H29N3O2S (1401113-29-8)

Guidance literature:

With tetra(n-butyl)ammonium hydroxide; In tetrahydrofuran; at 60 ℃; for 5h; Inert atmosphere;

DOI:10.1016/j.jpcs.2012.04.008

Reference yield:

10H-phenothiazine (92-84-2) → C29H29N3O2S (1401113-29-8)

Guidance literature:

Multi-step reaction with 3 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / Cooling with ice

1.2: 4 h / 20 °C

2.1: trichlorophosphate / 4 h / 0 - 70 °C / Inert atmosphere

3.1: tetra(n-butyl)ammonium hydroxide / tetrahydrofuran / 5 h / 60 °C / Inert atmosphere

With tetra(n-butyl)ammonium hydroxide; sodium hydride; trichlorophosphate; In tetrahydrofuran; N,N-dimethyl-formamide; 2.1: Vilsmeier formylation / 3.1: Knoevenagel condensation;

DOI:10.1016/j.jpcs.2012.04.008

Reference yield:

3-bromomethylheptane (18908-66-2) → C29H29N3O2S (1401113-29-8)

Guidance literature:

Multi-step reaction with 3 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / Cooling with ice

1.2: 4 h / 20 °C

2.1: trichlorophosphate / 4 h / 0 - 70 °C / Inert atmosphere

3.1: tetra(n-butyl)ammonium hydroxide / tetrahydrofuran / 5 h / 60 °C / Inert atmosphere

With tetra(n-butyl)ammonium hydroxide; sodium hydride; trichlorophosphate; In tetrahydrofuran; N,N-dimethyl-formamide; 2.1: Vilsmeier formylation / 3.1: Knoevenagel condensation;

DOI:10.1016/j.jpcs.2012.04.008

upstream raw materials:

3-bromomethylheptane

10H-phenothiazine

4-Nitrophenylacetonitrile

10-(2-ethylhexyl)-10H-3-phenothiazine carbaldehyde