methyl (2R,3S)-2,3-dihydroxy-2,3-di-O-isopropylidene-3-(4-methylphenyl)propionate

Base Information

Chemical Name:methyl (2R,3S)-2,3-dihydroxy-2,3-di-O-isopropylidene-3-(4-methylphenyl)propionate
CAS No.:351340-32-4
Molecular Formula:C₁₄H₁₈O₄
Molecular Weight:250.295
Hs Code.:

Synonyms:methyl (2R,3S)-2,3-dihydroxy-2,3-di-O-isopropylidene-3-(4-methylphenyl)propionate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl (2R,3S)-2,3-dihydroxy-2,3-di-O-isopropylidene-3-(4-methylphenyl)propionate

Chemical Property:

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Technology Process of methyl (2R,3S)-2,3-dihydroxy-2,3-di-O-isopropylidene-3-(4-methylphenyl)propionate

There total 2 articles about methyl (2R,3S)-2,3-dihydroxy-2,3-di-O-isopropylidene-3-(4-methylphenyl)propionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 77-76-9
2,2-dimethoxy-propane

: 206346-42-1
methyl (2R,3S)-2,3-dihydroxy-3-(4'-methylphenyl)propanoate

: 351340-32-4
methyl (2R,3S)-2,3-dihydroxy-2,3-di-O-isopropylidene-3-(4-methylphenyl)propionate

Guidance literature:: With toluene-4-sulfonic acid; In benzene; for 1h; Heating;
DOI:10.1021/jo990964c

Reference yield:

: 20754-20-5
3-p-tolyl-acrylic acid methyl ester

: 351340-32-4
methyl (2R,3S)-2,3-dihydroxy-2,3-di-O-isopropylidene-3-(4-methylphenyl)propionate

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / K₂OsO₂(OH)4; (DHQ)2-PHAL; K₃Fe(CN)6 / K₂CO₃; methanesulfonamide / H₂O; 2-methyl-propan-2-ol / 20 °C

2: 90 percent / p-TsOH*H₂O / benzene / 1 h / Heating

With potassium dioxotetrahydroxoosmate(VI); (DHQ)2-PHAL; toluene-4-sulfonic acid; potassium hexacyanoferrate(III); methanesulfonamide; potassium carbonate; In water; tert-butyl alcohol; benzene; 1: Sharpless AD reaction / 2: Cycloaddition;
DOI:10.1021/jo990964c