n-butyl-phenylphosphinothioic acid

Base Information

• Chemical Name: n-butyl-phenylphosphinothioic acid
• CAS No.: 18629-28-2
• Molecular Formula: C₁₀H₁₅OPS
• Molecular Weight: 214.268

Synonyms:n-butyl-phenylphosphinothioic acid

Chemical Property of n-butyl-phenylphosphinothioic acid

Chemical Property:

Purity/Quality:

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Technology Process of n-butyl-phenylphosphinothioic acid

There total 4 articles about n-butyl-phenylphosphinothioic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

butyl phenylphosphinate (6172-81-2) → n-butyl-phenylphosphinothioic acid (18629-28-2)

Guidance literature:

butyl phenylphosphinate; With n-butyllithium; In diethyl ether; hexane; at -78 - 20 ℃; for 3h; Inert atmosphere;

With sulfur; In diethyl ether; hexane; at 20 ℃; Inert atmosphere;

DOI:10.1021/acs.joc.0c01151

Reference yield:

C11H17O3PS2 → (R)-Butyl-phenyl-phosphinothioic acid (18629-28-2)

Guidance literature:

With water; In acetone;

DOI:10.1021/ja00547a044

Reference yield:

(S)-Butyl-phenyl-phosphinothioic acid (18629-28-2) → (R)-Butyl-phenyl-phosphinothioic acid (18629-28-2)

Guidance literature:

Multi-step reaction with 2 steps

1: triethylamine

2: water / acetone

With water; triethylamine; In acetone;

DOI:10.1021/ja00547a044

upstream raw materials:

butyl phenylphosphinate

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