methyl (2S)-4-amino-2-({[1-(diphenylmethyl)-2-oxo-1,2-dihydropyridin-3-yl]carbonyl}amino)butanoate trifluoroacetate

Base Information

• Chemical Name: methyl (2S)-4-amino-2-({[1-(diphenylmethyl)-2-oxo-1,2-dihydropyridin-3-yl]carbonyl}amino)butanoate trifluoroacetate
• CAS No.: 1037088-33-7
• Molecular Formula: C₂HF₃O₂*C₂₄H₂₅N₃O₄
• Molecular Weight: 533.504

Synonyms:methyl (2S)-4-amino-2-({[1-(diphenylmethyl)-2-oxo-1,2-dihydropyridin-3-yl]carbonyl}amino)butanoate trifluoroacetate

Chemical Property of methyl (2S)-4-amino-2-({[1-(diphenylmethyl)-2-oxo-1,2-dihydropyridin-3-yl]carbonyl}amino)butanoate trifluoroacetate

Chemical Property:

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Technology Process of methyl (2S)-4-amino-2-({[1-(diphenylmethyl)-2-oxo-1,2-dihydropyridin-3-yl]carbonyl}amino)butanoate trifluoroacetate

There total 1 articles about methyl (2S)-4-amino-2-({[1-(diphenylmethyl)-2-oxo-1,2-dihydropyridin-3-yl]carbonyl}amino)butanoate trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

methyl (2S)-4-[(tert-butoxycarbonyl)amino]-2-({[1-(diphenylmethyl)-2-oxo-1,2-dihydropyridin-3-yl]carbonyl}amino)butanoate (1037088-29-1) + trifluoroacetic acid (76-05-1) → methyl (2S)-4-amino-2-({[1-(diphenylmethyl)-2-oxo-1,2-dihydropyridin-3-yl]carbonyl}amino)butanoate trifluoroacetate (1037088-33-7)

Guidance literature:

With triethylsilane; water; at 20 ℃; for 2.5h; Product distribution / selectivity;

Reference yield: 98.0%

ethoxycarbonyl isothiourea (3673-38-9) + methyl (2S)-4-amino-2-({[1-(diphenylmethyl)-2-oxo-1,2-dihydropyridin-3-yl]carbonyl}amino)butanoate trifluoroacetate (1037088-33-7) → methyl (2S)-2-({[1-(diphenylmethyl)-2-oxo-1,2-dihydropyridin-3-yl]carbonyl}amino)-4-{[(ethoxycarbonyl)carbamothioyl]amino}butanoate (1037088-41-7)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 0.0833333h;

Reference yield: 48.0%

methyl (2S)-4-amino-2-({[1-(diphenylmethyl)-2-oxo-1,2-dihydropyridin-3-yl]carbonyl}amino)butanoate trifluoroacetate (1037088-33-7) + methyl N-[(2,2,5,7,8-pentamethyl-3,4-dihydro-2H-chromen-6-yl)sulfonyl]imidothiocarbamate (185674-98-0) → methyl (2S)-2-({[1-(diphenylmethyl)-2-oxo-1,2-dihydropyridin-3-yl]carbonyl}amino)-4-{[(2,2,5,7,8-pentamethyl-3,4-dihydro-2H-chromen-6-yl)sulfonyl]carbamimidamido}butanoate (1037088-35-9)

Guidance literature:

With mercury(I) perchlorate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; for 4h; Heating / reflux;

upstream raw materials:

methyl (2S)-4-[(tert-butoxycarbonyl)amino]-2-({[1-(diphenylmethyl)-2-oxo-1,2-dihydropyridin-3-yl]carbonyl}amino)butanoate

trifluoroacetic acid

Downstream raw materials:

methyl (2S)-2-({[1-(diphenylmethyl)-2-oxo-1,2-dihydropyridin-3-yl]carbonyl}amino)-4-{[(2,2,5,7,8-pentamethyl-3,4-dihydro-2H-chromen-6-yl)sulfonyl]carbamimidamido}butanoate

methyl (2S)-2-({[1-(diphenylmethyl)-2-oxo-1,2-dihydropyridin-3-yl]carbonyl}amino)-4-{[(ethoxycarbonyl)carbamothioyl]amino}butanoate

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