3,5-dichloro-2-methoxybenzenesulfonic acid 3-[2-(4-cyanophenyl)ethoxy]phenyl ester

Base Information

Chemical Name:3,5-dichloro-2-methoxybenzenesulfonic acid 3-[2-(4-cyanophenyl)ethoxy]phenyl ester
CAS No.:372523-08-5
Molecular Formula:C₂₂H₁₇Cl₂NO₅S
Molecular Weight:478.353
Hs Code.:

Synonyms:3,5-dichloro-2-methoxybenzenesulfonic acid 3-[2-(4-cyanophenyl)ethoxy]phenyl ester

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Chemical Property of 3,5-dichloro-2-methoxybenzenesulfonic acid 3-[2-(4-cyanophenyl)ethoxy]phenyl ester

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Technology Process of 3,5-dichloro-2-methoxybenzenesulfonic acid 3-[2-(4-cyanophenyl)ethoxy]phenyl ester

There total 3 articles about 3,5-dichloro-2-methoxybenzenesulfonic acid 3-[2-(4-cyanophenyl)ethoxy]phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

: 69395-13-7
4-(2-hydroxyethyl)benzonitrile

: 372522-97-9
3,5-dichloro-2-methoxybenzenesulfonic acid 3-hydroxyphenyl ester

: 372523-08-5
3,5-dichloro-2-methoxybenzenesulfonic acid 3-[2-(4-cyanophenyl)ethoxy]phenyl ester

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; at 20 ℃; for 16h;
DOI:10.1021/jm010833f

Reference yield:

: 19116-94-0
3,5-dichloro-2-methoxybenzene-1-sulfonyl chloride

: 372523-08-5
3,5-dichloro-2-methoxybenzenesulfonic acid 3-[2-(4-cyanophenyl)ethoxy]phenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 23 percent / aq. NaHCO₃ / diethyl ether / 48 h / 20 °C

2: 25 percent / DEAD; PPh₃ / tetrahydrofuran / 16 h / 20 °C

With sodium hydrogencarbonate; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; diethyl ether; 2: Mitsunobu reaction;
DOI:10.1021/jm010833f

Reference yield:

: 108-46-3
recorcinol

: 372523-08-5
3,5-dichloro-2-methoxybenzenesulfonic acid 3-[2-(4-cyanophenyl)ethoxy]phenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 23 percent / aq. NaHCO₃ / diethyl ether / 48 h / 20 °C

2: 25 percent / DEAD; PPh₃ / tetrahydrofuran / 16 h / 20 °C

With sodium hydrogencarbonate; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; diethyl ether; 2: Mitsunobu reaction;
DOI:10.1021/jm010833f