C₁₄H₁₃F₅N₂O

Base Information

Chemical Name:C₁₄H₁₃F₅N₂O
CAS No.:953077-41-3
Molecular Formula:C₁₄H₁₃F₅N₂O
Molecular Weight:320.262
Hs Code.:

C<sub>14</sub>H<sub>13</sub>F<sub>5</sub>N<sub>2</sub>O

Synonyms:C₁₄H₁₃F₅N₂O

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Chemical Property of C₁₄H₁₃F₅N₂O

Chemical Property:

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Technology Process of C₁₄H₁₃F₅N₂O

There total 7 articles about C₁₄H₁₃F₅N₂O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 953081-38-4
C₁₀H₉ClF₂O

: 953077-41-3
C₁₄H₁₃F₅N₂O

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium hydroxide / water; toluene / 4 h / 20 °C

2.1: sodium ethanolate / palladium diacetate; 1,2-bis-(diphenylphosphino)ethane / toluene / 6.25 - 10.25 h / 20 - 25 °C

3.1: triethylamine / toluene / 0.5 h / 3 °C

4.1: lithium bromide / ISOPROPYLAMIDE / 13 h / 28 - 30 °C

5.1: water; lithium chloride / ISOPROPYLAMIDE / 12 - 14 h / 113 - 115 °C

6.1: trifluoroacetic acid / toluene / 12 - 15 h / 85 - 90 °C

6.2: 20 °C

7.1: hydrogenchloride / 1,4-dioxane / 12 h / 85 °C

7.2: pH 8 - 10

With hydrogenchloride; sodium hydroxide; water; sodium ethanolate; triethylamine; trifluoroacetic acid; lithium chloride; palladium diacetate; 1,2-bis-(diphenylphosphino)ethane; lithium bromide; In 1,4-dioxane; ISOPROPYLAMIDE; water; toluene;

Reference yield:

: 953077-38-8
2-(2,3-difluorophenyl)-2-vinyloxirane

: 953077-41-3
C₁₄H₁₃F₅N₂O

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium ethanolate / palladium diacetate; 1,2-bis-(diphenylphosphino)ethane / toluene / 6.25 - 10.25 h / 20 - 25 °C

2.1: triethylamine / toluene / 0.5 h / 3 °C

3.1: lithium bromide / ISOPROPYLAMIDE / 13 h / 28 - 30 °C

4.1: water; lithium chloride / ISOPROPYLAMIDE / 12 - 14 h / 113 - 115 °C

5.1: trifluoroacetic acid / toluene / 12 - 15 h / 85 - 90 °C

5.2: 20 °C

6.1: hydrogenchloride / 1,4-dioxane / 12 h / 85 °C

6.2: pH 8 - 10

With hydrogenchloride; water; sodium ethanolate; triethylamine; trifluoroacetic acid; lithium chloride; palladium diacetate; 1,2-bis-(diphenylphosphino)ethane; lithium bromide; In 1,4-dioxane; ISOPROPYLAMIDE; toluene;

Reference yield:

: 929249-82-1
2-chloro-1-(2,3-difluorophenyl)ethan-1-one

: 953077-41-3
C₁₄H₁₃F₅N₂O

Guidance literature:: Multi-step reaction with 8 steps

1.1: tetrahydrofuran; toluene / -60 - 0 °C

2.1: sodium hydroxide / water; toluene / 4 h / 20 °C

3.1: sodium ethanolate / palladium diacetate; 1,2-bis-(diphenylphosphino)ethane / toluene / 6.25 - 10.25 h / 20 - 25 °C

4.1: triethylamine / toluene / 0.5 h / 3 °C

5.1: lithium bromide / ISOPROPYLAMIDE / 13 h / 28 - 30 °C

6.1: water; lithium chloride / ISOPROPYLAMIDE / 12 - 14 h / 113 - 115 °C

7.1: trifluoroacetic acid / toluene / 12 - 15 h / 85 - 90 °C

7.2: 20 °C

8.1: hydrogenchloride / 1,4-dioxane / 12 h / 85 °C

8.2: pH 8 - 10

With hydrogenchloride; sodium hydroxide; water; sodium ethanolate; triethylamine; trifluoroacetic acid; lithium chloride; palladium diacetate; 1,2-bis-(diphenylphosphino)ethane; lithium bromide; In tetrahydrofuran; 1,4-dioxane; ISOPROPYLAMIDE; water; toluene;