(S)-2-tert-butoxycarbonylamino-3,3-dimethyl-3-(4,6-dimethyl-2-hydroxyphenyl)propanol tert-butyldimethylsilyl ether

Base Information

Chemical Name:(S)-2-tert-butoxycarbonylamino-3,3-dimethyl-3-(4,6-dimethyl-2-hydroxyphenyl)propanol tert-butyldimethylsilyl ether
CAS No.:1250254-53-5
Molecular Formula:C₂₄H₄₃NO₄Si
Molecular Weight:437.695
Hs Code.:

Synonyms:(S)-2-tert-butoxycarbonylamino-3,3-dimethyl-3-(4,6-dimethyl-2-hydroxyphenyl)propanol tert-butyldimethylsilyl ether

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Chemical Property of (S)-2-tert-butoxycarbonylamino-3,3-dimethyl-3-(4,6-dimethyl-2-hydroxyphenyl)propanol tert-butyldimethylsilyl ether

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Technology Process of (S)-2-tert-butoxycarbonylamino-3,3-dimethyl-3-(4,6-dimethyl-2-hydroxyphenyl)propanol tert-butyldimethylsilyl ether

There total 1 articles about (S)-2-tert-butoxycarbonylamino-3,3-dimethyl-3-(4,6-dimethyl-2-hydroxyphenyl)propanol tert-butyldimethylsilyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1250254-51-3
(S)-3-(2-benzyloxy-4,6-dimethylphenyl)-2-tert-butoxycarbonylamino-3,3-dimethylpropanol tert-butyldimethylsilyl ether

: 1250254-53-5
(S)-2-tert-butoxycarbonylamino-3,3-dimethyl-3-(4,6-dimethyl-2-hydroxyphenyl)propanol tert-butyldimethylsilyl ether

Guidance literature:: With 1% Pd/C; hydrogen; sodium hydrogencarbonate; In methanol;
DOI:10.1016/j.tet.2010.07.033

Reference yield: 98.0%

: 1250254-53-5
(S)-2-tert-butoxycarbonylamino-3,3-dimethyl-3-(4,6-dimethyl-2-hydroxyphenyl)propanol tert-butyldimethylsilyl ether

: 116748-06-2
(4-(hydroxymethyl)phenoxy)(tert-butyl)diphenylsilane

: (S)-tert-butyl [1-{(tert-butyldimethylsilyl)oxy}-3-{2-([4-{(tert-butyldiphenylsilyl)oxy}benzyl]oxy)-4,6-dimethylphenyl}-3-methylbutan-2-yl]carbamate

Guidance literature:: With tributylphosphine; diamide; In toluene; at 0 - 20 ℃; for 3.5h; Inert atmosphere;
DOI:10.1016/j.tet.2014.05.110

Reference yield: 92.0%

: 1250254-53-5
(S)-2-tert-butoxycarbonylamino-3,3-dimethyl-3-(4,6-dimethyl-2-hydroxyphenyl)propanol tert-butyldimethylsilyl ether

: 2-{4-(chloromethyl)phenyl}-6-methyl-1,3,6,2-dioxazaborocane-4,8-dione

: (S)-tert-butyl [1-{(tert-butyldimethylsilyl)oxy}-3-(2,4-dimethyl-6-[{4-(6-methyl-4,8-dioxo-1,3,6,2-dioxazaborocan-2-yl)benzyl}oxy]phenyl)-3-methylbutan-2-yl]carbamate

Guidance literature:: With potassium carbonate; potassium iodide; In N,N-dimethyl-formamide; for 48h; Inert atmosphere;
DOI:10.1016/j.tetlet.2015.05.060