(S)-2-tert-butoxycarbonylamino-3,3-dimethyl-3-[2,4-dimethyl-6-(nitrobenzene-4-sulfonyloxy)phenyl]propanol tert-butyldimethylsilyl ether

Base Information

Chemical Name:(S)-2-tert-butoxycarbonylamino-3,3-dimethyl-3-[2,4-dimethyl-6-(nitrobenzene-4-sulfonyloxy)phenyl]propanol tert-butyldimethylsilyl ether
CAS No.:1643392-46-4
Molecular Formula:C₃₀H₄₆N₂O₈SSi
Molecular Weight:622.855
Hs Code.:

Synonyms:(S)-2-tert-butoxycarbonylamino-3,3-dimethyl-3-[2,4-dimethyl-6-(nitrobenzene-4-sulfonyloxy)phenyl]propanol tert-butyldimethylsilyl ether

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Chemical Property of (S)-2-tert-butoxycarbonylamino-3,3-dimethyl-3-[2,4-dimethyl-6-(nitrobenzene-4-sulfonyloxy)phenyl]propanol tert-butyldimethylsilyl ether

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Technology Process of (S)-2-tert-butoxycarbonylamino-3,3-dimethyl-3-[2,4-dimethyl-6-(nitrobenzene-4-sulfonyloxy)phenyl]propanol tert-butyldimethylsilyl ether

There total 1 articles about (S)-2-tert-butoxycarbonylamino-3,3-dimethyl-3-[2,4-dimethyl-6-(nitrobenzene-4-sulfonyloxy)phenyl]propanol tert-butyldimethylsilyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1250254-53-5
(S)-2-tert-butoxycarbonylamino-3,3-dimethyl-3-(4,6-dimethyl-2-hydroxyphenyl)propanol tert-butyldimethylsilyl ether

: 98-74-8
4-Nitrobenzenesulfonyl chloride

: 1643392-46-4
(S)-2-tert-butoxycarbonylamino-3,3-dimethyl-3-[2,4-dimethyl-6-(nitrobenzene-4-sulfonyloxy)phenyl]propanol tert-butyldimethylsilyl ether

Guidance literature:: With potassium carbonate; In acetone; Inert atmosphere;
DOI:10.1039/c4ob00622d

Reference yield: 92.0%

: 1643392-46-4
(S)-2-tert-butoxycarbonylamino-3,3-dimethyl-3-[2,4-dimethyl-6-(nitrobenzene-4-sulfonyloxy)phenyl]propanol tert-butyldimethylsilyl ether

: 1643392-47-5
(S)-2-tert-butoxycarbonylamino-3,3-dimethyl-3-[2,4-dimethyl-6-(nitrobenzene-4-sulfonyloxy)phenyl]propanol

Guidance literature:: With acetic acid; In tetrahydrofuran; water; Inert atmosphere;
DOI:10.1039/c4ob00622d

Reference yield:

: 1643392-46-4
(S)-2-tert-butoxycarbonylamino-3,3-dimethyl-3-[2,4-dimethyl-6-(nitrobenzene-4-sulfonyloxy)phenyl]propanol tert-butyldimethylsilyl ether

: C₂₄H₃₀N₂O₉S

Guidance literature:: Multi-step reaction with 3 steps

1: acetic acid / water; tetrahydrofuran / Inert atmosphere

2: dipyridinium dichromate / N,N-dimethyl-formamide / Inert atmosphere

3: sodium chlorite; 2-methyl-but-2-ene; sodium dihydrogenphosphate / acetone; water; tert-butyl alcohol / Inert atmosphere

With sodium chlorite; sodium dihydrogenphosphate; dipyridinium dichromate; 2-methyl-but-2-ene; acetic acid; In tetrahydrofuran; water; N,N-dimethyl-formamide; acetone; tert-butyl alcohol;
DOI:10.1039/c4ob00622d