3-(dibenzo[b,d]furan-4-yl)-9-(4,6-diphenyl-1,3,5-triazin-2-yl)-9H-carbazole

Base Information

Chemical Name:3-(dibenzo[b,d]furan-4-yl)-9-(4,6-diphenyl-1,3,5-triazin-2-yl)-9H-carbazole
CAS No.:1346669-12-2
Molecular Formula:C₃₉H₂₄N₄O
Molecular Weight:564.646
Hs Code.:

Synonyms:3-(dibenzo[b,d]furan-4-yl)-9-(4,6-diphenyl-1,3,5-triazin-2-yl)-9H-carbazole

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Chemical Property of 3-(dibenzo[b,d]furan-4-yl)-9-(4,6-diphenyl-1,3,5-triazin-2-yl)-9H-carbazole

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Technology Process of 3-(dibenzo[b,d]furan-4-yl)-9-(4,6-diphenyl-1,3,5-triazin-2-yl)-9H-carbazole

There total 4 articles about 3-(dibenzo[b,d]furan-4-yl)-9-(4,6-diphenyl-1,3,5-triazin-2-yl)-9H-carbazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.5%

: 3842-55-5
2-chloro-4,6-diphenyl-1,3,5-triazine

: 1346669-46-2
3-(dibenzo[b,d]furan-4-yl)-9H-carbazole

: 1346669-12-2
3-(dibenzo[b,d]furan-4-yl)-9-(4,6-diphenyl-1,3,5-triazin-2-yl)-9H-carbazole

Guidance literature:: 3-(dibenzo[b,d]furan-4-yl)-9H-carbazole; With sodium hydride; In N,N-dimethyl-formamide; for 0.25h; Inert atmosphere;

2-chloro-4,6-diphenyl-1,3,5-triazine; In N,N-dimethyl-formamide; at 20 ℃; Inert atmosphere;
DOI:10.1039/c6ra27770e

Reference yield:

: 89827-45-2
4-bromodibenzofuran

: 9-(4,6-diphenyl-1,3,5-triazin-2-yl)-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-9H-carbazole

: 1346669-12-2
3-(dibenzo[b,d]furan-4-yl)-9-(4,6-diphenyl-1,3,5-triazin-2-yl)-9H-carbazole

Guidance literature:: With bis(tri-t-butylphosphine)palladium⁽⁰⁾; sodium t-butanolate; In toluene; for 6h; Reflux; Inert atmosphere;

Reference yield:

: 1592-95-6
3-bromo-9H-carbazole

: 1346669-12-2
3-(dibenzo[b,d]furan-4-yl)-9-(4,6-diphenyl-1,3,5-triazin-2-yl)-9H-carbazole

Guidance literature:: Multi-step reaction with 2 steps

1.1: palladium diacetate; potassium carbonate; 2-di-t-butylphosphino-3,4,5,6-tetramethyl-2',4',6'-tri-1-propylbiphenyl / tetrahydrofuran / 4 h / 70 °C / Inert atmosphere

2.1: sodium hydride / N,N-dimethyl-formamide / 0.25 h / Inert atmosphere

2.2: 20 °C / Inert atmosphere

With 2-di-t-butylphosphino-3,4,5,6-tetramethyl-2',4',6'-tri-1-propylbiphenyl; palladium diacetate; sodium hydride; potassium carbonate; In tetrahydrofuran; N,N-dimethyl-formamide; 1.1: |Suzuki Coupling;
DOI:10.1039/c6ra27770e