C₂₆H₂₂OS₃

Base Information

• Chemical Name: C₂₆H₂₂OS₃
• CAS No.: 131376-21-1
• Molecular Formula: C₂₆H₂₂OS₃
• Molecular Weight: 446.658
• Mol file: 131376-21-1.mol

Synonyms:C₂₆H₂₂OS₃

Chemical Property of C₂₆H₂₂OS₃

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of C₂₆H₂₂OS₃

There total 4 articles about C₂₆H₂₂OS₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

para-thiocresol (106-45-6) + 5-(p-anisyl)thianthrenium bromide → 4-methylphenyl 4-methoxyphenyl sulfide (6013-47-4) + C26H22OS3 (131376-21-1)

Guidance literature:

para-thiocresol; With sodium; In diethyl ether; Heating;

5-(p-anisyl)thianthrenium bromide; In acetonitrile; at 20 ℃;

DOI:10.1002/poc.462

Reference yield: 92.0%

5-(4-anisyl)thianthreniumyl perchlorate + para-thiocresol (106-45-6) → C26H22OS3 (131376-21-1)

Guidance literature:

With sodium hydride; In tetrahydrofuran; for 2.5h; Ambient temperature;

DOI:10.1016/S0040-4039(00)97918-8

Reference yield:

thianthrene-5-oxide (2362-50-7) → C26H22OS3 (131376-21-1)

Guidance literature:

Multi-step reaction with 2 steps

1.1: 69 percent / benzene / Heating

2.1: Na / diethyl ether / Heating

2.2: 94 percent / acetonitrile / 20 °C

With sodium; In diethyl ether; benzene;

DOI:10.1002/poc.462

upstream raw materials:

para-thiocresol

thianthrene-5-oxide

4-methoxyphenyl magnesium bromide