benzyl 3-(3-(3,4-bis(benzyloxy)phenyl)propanamido)propyl(4-aminobutyl)carbamate

Base Information

Chemical Name:benzyl 3-(3-(3,4-bis(benzyloxy)phenyl)propanamido)propyl(4-aminobutyl)carbamate
CAS No.:1375180-09-8
Molecular Formula:C₃₈H₄₅N₃O₅
Molecular Weight:623.792
Hs Code.:

Synonyms:benzyl 3-(3-(3,4-bis(benzyloxy)phenyl)propanamido)propyl(4-aminobutyl)carbamate

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Chemical Property of benzyl 3-(3-(3,4-bis(benzyloxy)phenyl)propanamido)propyl(4-aminobutyl)carbamate

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Technology Process of benzyl 3-(3-(3,4-bis(benzyloxy)phenyl)propanamido)propyl(4-aminobutyl)carbamate

There total 8 articles about benzyl 3-(3-(3,4-bis(benzyloxy)phenyl)propanamido)propyl(4-aminobutyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1375180-08-7
C₄₃H₅₃N₃O₇

: 1375180-09-8
benzyl 3-(3-(3,4-bis(benzyloxy)phenyl)propanamido)propyl(4-aminobutyl)carbamate

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 20 ℃;

Reference yield:

: 68076-40-4
N¹-tert-butoxycarbonyl-N⁴-(2-cyanoethyl)-1,4-butanediamine

: 1375180-09-8
benzyl 3-(3-(3,4-bis(benzyloxy)phenyl)propanamido)propyl(4-aminobutyl)carbamate

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine / tetrahydrofuran / 20 °C

2: ammonia; hydrogen / methanol / 50 °C / 37503.8 - 75007.5 Torr / Autoclave

3: triethylamine / dichloromethane / 0 °C

4: trifluoroacetic acid / dichloromethane / 20 °C

With ammonia; hydrogen; triethylamine; trifluoroacetic acid; In tetrahydrofuran; methanol; dichloromethane;

Reference yield:

: 2107-70-2
3,4-methoxycinnamic acid

: 1375180-09-8
benzyl 3-(3-(3,4-bis(benzyloxy)phenyl)propanamido)propyl(4-aminobutyl)carbamate

Guidance literature:: Multi-step reaction with 6 steps

1: water; hydrogen bromide / 140 °C

2: potassium carbonate / N,N-dimethyl-formamide / 80 °C

3: sodium hydroxide; water / methanol / 90 °C / Reflux

4: thionyl chloride; N,N-dimethyl-formamide / dichloromethane / 5 h / 20 - 65 °C / Reflux

5: triethylamine / dichloromethane / 0 °C

6: trifluoroacetic acid / dichloromethane / 20 °C

With thionyl chloride; water; hydrogen bromide; potassium carbonate; triethylamine; N,N-dimethyl-formamide; trifluoroacetic acid; sodium hydroxide; In methanol; dichloromethane; N,N-dimethyl-formamide;