diethyl N-<5-amino-1-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)imidazole-4-sulfonyl>-L-aspartate

Base Information

Chemical Name:diethyl N-<5-amino-1-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)imidazole-4-sulfonyl>-L-aspartate
CAS No.:179999-15-6
Molecular Formula:C₃₇H₃₈N₄O₁₃S
Molecular Weight:778.794
Hs Code.:

Synonyms:diethyl N-<5-amino-1-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)imidazole-4-sulfonyl>-L-aspartate

Suppliers and Price of diethyl N-<5-amino-1-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)imidazole-4-sulfonyl>-L-aspartate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of diethyl N-<5-amino-1-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)imidazole-4-sulfonyl>-L-aspartate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of diethyl N-<5-amino-1-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)imidazole-4-sulfonyl>-L-aspartate

There total 4 articles about diethyl N-<5-amino-1-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)imidazole-4-sulfonyl>-L-aspartate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 161359-36-0
diethyl N-<5-nitro-1-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)imidazole-5-sulfonyl>-L-aspartate

: 179999-15-6
diethyl N-<5-amino-1-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)imidazole-4-sulfonyl>-L-aspartate

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethyl acetate;
DOI:10.1080/15257779508012383

Reference yield:

: 6974-32-9
1-O-acetyl-2,3,5-tri-O-benzoyl-β-D-ribofuranose

: 179999-15-6
diethyl N-<5-amino-1-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)imidazole-4-sulfonyl>-L-aspartate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) chlorotrimethylsilane, hexamethyldisilazane, 2.) trimethylsilyl trifluoromethanesulfonate / 1.) xylene, 130 deg C, 90 min, 2.) acetonitrile, RT, 3 min

2: 96 percent / H₂ / 5percent Pd/C / ethyl acetate / 760 Torr

With chloro-trimethyl-silane; trimethylsilyl trifluoromethanesulfonate; hydrogen; 1,1,1,3,3,3-hexamethyl-disilazane; palladium on activated charcoal; In ethyl acetate;
DOI:10.1016/0040-4020(96)00472-3

Reference yield:

: 161359-34-8
diethyl N-<4(5)-nitroimidazole-5(4)-sulphonyl>-L-aspartate

: 179999-15-6
diethyl N-<5-amino-1-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)imidazole-4-sulfonyl>-L-aspartate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) chlorotrimethylsilane, hexamethyldisilazane, 2.) trimethylsilyl trifluoromethanesulfonate / 1.) xylene, 130 deg C, 90 min, 2.) acetonitrile, RT, 3 min

2: 96 percent / H₂ / 5percent Pd/C / ethyl acetate / 760 Torr

With chloro-trimethyl-silane; trimethylsilyl trifluoromethanesulfonate; hydrogen; 1,1,1,3,3,3-hexamethyl-disilazane; palladium on activated charcoal; In ethyl acetate;
DOI:10.1016/0040-4020(96)00472-3