7-(3,5-Di-tert-butylphenyl)-2,12-bis(4-methoxyacridin-9-yl)-5,6,8,9-tetrahydrodibenzacridine

Base Information

• Chemical Name: 7-(3,5-Di-tert-butylphenyl)-2,12-bis(4-methoxyacridin-9-yl)-5,6,8,9-tetrahydrodibenzacridine
• CAS No.: 118656-24-9
• Molecular Formula: C₆₃H₅₅N₃O₂
• Molecular Weight: 886.149

Synonyms:7-(3,5-Di-tert-butylphenyl)-2,12-bis(4-methoxyacridin-9-yl)-5,6,8,9-tetrahydrodibenzacridine

Chemical Property of 7-(3,5-Di-tert-butylphenyl)-2,12-bis(4-methoxyacridin-9-yl)-5,6,8,9-tetrahydrodibenzacridine

Chemical Property:

Purity/Quality:

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Technology Process of 7-(3,5-Di-tert-butylphenyl)-2,12-bis(4-methoxyacridin-9-yl)-5,6,8,9-tetrahydrodibenzacridine

There total 7 articles about 7-(3,5-Di-tert-butylphenyl)-2,12-bis(4-methoxyacridin-9-yl)-5,6,8,9-tetrahydrodibenzacridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

7-bromo-3,4-dihydro-2H-naphthalen-1-one (32281-97-3) → 7-(3,5-Di-tert-butylphenyl)-2,12-bis(4-methoxyacridin-9-yl)-5,6,8,9-tetrahydrodibenzacridine (118656-24-9)

Guidance literature:

Multi-step reaction with 5 steps

1: 92 percent / p-toluenesulfonic acid / toluene / 12 h / Heating

3: 62 percent / 4percent KOH / methanol / 2.75 h / 75 °C

4: 1.) 70percent perchloric acid / 1.) 70 deg C, 4 h, 2.) C₂H₅OH

5: NH₃ / methanol; CH₂Cl₂

With potassium hydroxide; perchloric acid; ammonia; toluene-4-sulfonic acid; In methanol; dichloromethane; toluene;

DOI:10.1021/ja00186a035

Reference yield:

7-Bromo-1,2,3,4-tetrahydronaphthalene-1-spiro-2'-(1',3'-dioxacyclopentane) (111773-13-8) → 7-(3,5-Di-tert-butylphenyl)-2,12-bis(4-methoxyacridin-9-yl)-5,6,8,9-tetrahydrodibenzacridine (118656-24-9)

Guidance literature:

Multi-step reaction with 4 steps

2: 62 percent / 4percent KOH / methanol / 2.75 h / 75 °C

3: 1.) 70percent perchloric acid / 1.) 70 deg C, 4 h, 2.) C₂H₅OH

4: NH₃ / methanol; CH₂Cl₂

With potassium hydroxide; perchloric acid; ammonia; In methanol; dichloromethane;

DOI:10.1021/ja00186a035

Reference yield:

7-(4-Methoxyacridin-9-yl)-1-oxo-1,2,3,4-tetrahydronaphthalene (118656-08-9) → 7-(3,5-Di-tert-butylphenyl)-2,12-bis(4-methoxyacridin-9-yl)-5,6,8,9-tetrahydrodibenzacridine (118656-24-9)

Guidance literature:

Multi-step reaction with 3 steps

1: 62 percent / 4percent KOH / methanol / 2.75 h / 75 °C

2: 1.) 70percent perchloric acid / 1.) 70 deg C, 4 h, 2.) C₂H₅OH

3: NH₃ / methanol; CH₂Cl₂

With potassium hydroxide; perchloric acid; ammonia; In methanol; dichloromethane;

DOI:10.1021/ja00186a035

upstream raw materials:

3,5-Di-tert-butylbenzaldehyde

7-bromo-3,4-dihydro-2H-naphthalen-1-one

7-Bromo-1,2,3,4-tetrahydronaphthalene-1-spiro-2'-(1',3'-dioxacyclopentane)

7-(4-Methoxyacridin-9-yl)-1-oxo-1,2,3,4-tetrahydronaphthalene

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