N-[(S)-3-((S)-4-Benzyl-2-oxo-oxazolidin-3-yl)-2-diazo-1-furan-2-yl-3-oxo-propyl]-4-methyl-benzenesulfonamide

Base Information

Chemical Name:N-[(S)-3-((S)-4-Benzyl-2-oxo-oxazolidin-3-yl)-2-diazo-1-furan-2-yl-3-oxo-propyl]-4-methyl-benzenesulfonamide
CAS No.:825627-52-9
Molecular Formula:C₂₄H₂₂N₄O₆S
Molecular Weight:494.528
Hs Code.:

Synonyms:N-[(S)-3-((S)-4-Benzyl-2-oxo-oxazolidin-3-yl)-2-diazo-1-furan-2-yl-3-oxo-propyl]-4-methyl-benzenesulfonamide

Suppliers and Price of N-[(S)-3-((S)-4-Benzyl-2-oxo-oxazolidin-3-yl)-2-diazo-1-furan-2-yl-3-oxo-propyl]-4-methyl-benzenesulfonamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-[(S)-3-((S)-4-Benzyl-2-oxo-oxazolidin-3-yl)-2-diazo-1-furan-2-yl-3-oxo-propyl]-4-methyl-benzenesulfonamide

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of N-[(S)-3-((S)-4-Benzyl-2-oxo-oxazolidin-3-yl)-2-diazo-1-furan-2-yl-3-oxo-propyl]-4-methyl-benzenesulfonamide

There total 3 articles about N-[(S)-3-((S)-4-Benzyl-2-oxo-oxazolidin-3-yl)-2-diazo-1-furan-2-yl-3-oxo-propyl]-4-methyl-benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 13707-47-6
2-furaldehyde tosylimine

: 825627-36-9
(S)-(-)-N-(α-diazo)acetyl-4-benzyl-2-oxazolidinone

: 825627-52-9
N-[(S)-3-((S)-4-Benzyl-2-oxo-oxazolidin-3-yl)-2-diazo-1-furan-2-yl-3-oxo-propyl]-4-methyl-benzenesulfonamide

: N-[(R)-3-((S)-4-Benzyl-2-oxo-oxazolidin-3-yl)-2-diazo-1-furan-2-yl-3-oxo-propyl]-4-methyl-benzenesulfonamide

Guidance literature:: With N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium; diisopropylamine; In tetrahydrofuran; hexane; at -98 ℃;
DOI:10.1002/anie.200460730

Reference yield:

: 90719-32-7
(S)-4-Benzyl-2-oxazolidinone

: 825627-52-9
N-[(S)-3-((S)-4-Benzyl-2-oxo-oxazolidin-3-yl)-2-diazo-1-furan-2-yl-3-oxo-propyl]-4-methyl-benzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: Et₃N / CH₂Cl₂ / -10 - 20 °C

1.2: 58 percent / CH₂Cl₂; diethyl ether / 4 h / cooling

2.1: n-BuLi; diisopropylamine; HMPA / tetrahydrofuran; hexane / -98 °C

With N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium; triethylamine; diisopropylamine; In tetrahydrofuran; hexane; dichloromethane;
DOI:10.1002/anie.200460730

Reference yield:

: 132836-66-9
(S)-3-acetyl-4-benzyloxazolidin-2-one

: 825627-52-9
N-[(S)-3-((S)-4-Benzyl-2-oxo-oxazolidin-3-yl)-2-diazo-1-furan-2-yl-3-oxo-propyl]-4-methyl-benzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: 50 percent / n-BuLi; diisopropylamine; o-nitrophenylsulfonyl azide / tetrahydrofuran; hexane / 5 h / -78 °C

2: n-BuLi; diisopropylamine; HMPA / tetrahydrofuran; hexane / -98 °C

With N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium; o-nitrobenzenesulfonyl azide; diisopropylamine; In tetrahydrofuran; hexane;
DOI:10.1002/anie.200460730